A general synthesis of phosphonic acid dichlorides using oxalyl chloride and DMF catalysis

作者: Roland S. Rogers

DOI: 10.1016/S0040-4039(00)60798-0

关键词:

摘要: Abstract A general synthesis of phosphonic diacid dichlorides ( 1 ) using oxalyl chloride and catalytic DMF is described.

参考文章(7)
Ludwig Maier, ORGANIC PHOSPHORUS COMPOUNDS 90.l A CONVENIENT, ONE-STEP SYNTHESIS OF ALKYL- AND ARYLPHOSPHONYL DICHLORIDES Phosphorus Sulfur and Silicon and The Related Elements. ,vol. 47, pp. 465- 470 ,(1990) , 10.1080/10426509008038002
G. O. Doak, Leon D. Freedman, The Preparation of Amides of Arylphosphonic Acids. I. Diamides of Primary Aromatic and Heterocyclic Amines1 Journal of the American Chemical Society. ,vol. 76, pp. 1621- 1623 ,(1954) , 10.1021/JA01635A046
Leon D. Freedman, Henry Tauber, G. O. Doak, Harold J. Magnuson, The Preparation of Some Organophosphorus Compounds Possessing Anticholinesterase Activity1 Journal of the American Chemical Society. ,vol. 75, pp. 1379- 1381 ,(1953) , 10.1021/JA01102A033
Helmut QUAST, Manfred HEUSCHMANN, Mohamed O. ABDEL-RAHMAN, Herstellung von Methylphosphonsäure-dichlorid Synthesis. ,vol. 1974, pp. 490- 490 ,(1974) , 10.1055/S-1974-23348