Alkylation of salts ofN-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides with alkyl halides and dimethyl sulfate
作者： O. A. Luk'yanov , G. A. Smirnov , S. V. Nikitin
DOI: 10.1007/BF02494502
关键词:
摘要: Salts ofN-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides, RCH(OH)CH2N(O)=NO− M+ (R=Me, Pri, or But; and M=Li, Na, K, Ag, NH4, Me4N), were prepared. Their alkylation with alkyl halides R′X (X=Cl, Br, I) dimethyl sulfate was studied. Generally, afforded mixtures ofN-(β-hydroxyalkyl)-N′-alkoxydiazeneN-oxides RCH(OH)CH2N(O)=NOR′ andO-alkyl-N-(β-hydroxyalkyl)-N-nitrosohydroxylamines RCH(OH)CH2N(NO)OR′.
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