Size-controlled synthesis of alumina nanoparticles from aluminum alkoxides

作者: Yong Kap Park , Erica H. Tadd , Melissa Zubris , Rina Tannenbaum

DOI: 10.1016/J.MATERRESBULL.2005.04.031

关键词:

摘要: Abstract Aluminum oxide nanoparticles were prepared by the hydrolysis of aluminum alkoxides followed calcinations, in presence surface stabilizing agents, such as Na(AOT) molecules. The size alumina precursors (bohemite) was 20–30 nm, yielding particles with an average 80 nm after calcinations at 1200 °C. shape α-alumina mainly spherical and high temperature inhibited formation hexagonal crystals. introduction during appropriate processing step, had effect controlling particles, degree aggregation shapes.

参考文章(23)
C. Jeffrey Brinker, George W. Scherer, Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing ,(1990)
H. Hofinann, J. Dutta, S. Scholz-Odermatt, R. Vacassy, J.-Ch. Valmalette, Potential of Nanosized Ceramic Powder for Functional Applications Westerville, OH, United States, 12 January 1997 through 16 January 1997, Cocoa, FL, USA. ,vol. 18, pp. 687- 694 ,(2008) , 10.1002/9780470294444.CH81
Gonzalo Gutiérrez, Adrian Taga, Börje Johansson, Theoretical structure determination of γ-Al 2 O 3 Physical Review B. ,vol. 65, pp. 012101- ,(2001) , 10.1103/PHYSREVB.65.012101
Zhen-Yan Deng, Takayuki Fukasawa, Motohide Ando, Guo-Jun Zhang, Tatsuki Ohji, Microstructure and Mechanical Properties of Porous Alumina Ceramics Fabricated by the Decomposition of Aluminum Hydroxide Journal of the American Ceramic Society. ,vol. 84, pp. 2638- 2644 ,(2001) , 10.1111/J.1151-2916.2001.TB01065.X
Mikhail Y. Lebedev, Michael V. Lauritzen, Albert E. Curzon, Steven Holdcroft, Solvato-Controlled Doping of Conducting Polymers Chemistry of Materials. ,vol. 10, pp. 156- 163 ,(1998) , 10.1021/CM970285N
V. Haas, R. Birringer, H. Gleiter, S.E. Pratsinis, Synthesis of nanostructured powders in an aerosol flow condenser Journal of Aerosol Science. ,vol. 28, pp. 1443- 1453 ,(1997) , 10.1016/S0021-8502(97)00006-2
A. J. Hoffman, G. Mills, H. Yee, M. R. Hoffmann, Q-sized cadmium sulfide: synthesis, characterization, and efficiency of photoinitiation of polymerization of several vinylic monomers The Journal of Physical Chemistry. ,vol. 96, pp. 5546- 5552 ,(1992) , 10.1021/J100192A067
X. Bokhimi, J.A. Toledo-Antonio, M.L. Guzmán-Castillo, B. Mar-Mar, F. Hernández-Beltrán, J. Navarrete, Dependence of Boehmite Thermal Evolution on Its Atom Bond Lengths and Crystallite Size Journal of Solid State Chemistry. ,vol. 161, pp. 319- 326 ,(2001) , 10.1006/JSSC.2001.9320
Matthew D. Curran, Thomas E. Gedris, A. E. Stiegman, Gary A. Plett, Synthetic Control over the Production of Multicomponent Sol−Gel Materials: Fabrication of Homogeneous Vanadia−Silica Xerogels with High Vanadium Content Chemistry of Materials. ,vol. 11, pp. 1120- 1127 ,(1999) , 10.1021/CM981119Y
Takashi Ogihara, Hidenori Nakajima, Teruaki Yanagawa, Nobuo Ogata, Kokichi Yoshida, Noritaka Matsushita, Preparation of monodisperse, spherical alumina powders from alkoxides Journal of the American Ceramic Society. ,vol. 74, pp. 2263- 2269 ,(1991) , 10.1111/J.1151-2916.1991.TB08294.X