Effect of Initial Reactants and Reaction Temperature on Molten Salt Synthesis of CuCo2O4 and Its Sustainable Energy Storage Properties

作者: M. V. Reddy , Mishra Rajesh , Stefan Adams , B. V. R. Chowdari

DOI: 10.1021/ACSSUSCHEMENG.6B00047

关键词:

摘要: We have prepared CuCo2O4 using 0.5 M NaNO3 and LiNO3 molten salts at different temperatures (410 610 °C) in the air. This was later used as an anode material for LIBs. The morphology, structure, electrochemical properties of products were observed various techniques such scanning electron microscopy, X-ray diffraction (XRD), Brunauer–Emmett–Teller surface density method, cyclic voltammetry, galvanostatic cycling tests. XRD patterns showed a minor CuO phase addition to major most reactant salt combination. copper sulfate cobalt °C acetate 410 best performance with capacities 848 mAh g–1 882 capacity retentions 93% 94%, respectively.

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