Batch‐injection versus Flow‐injection Analysis Using Screen‐printed Electrodes: Determination of Ciprofloxacin in Pharmaceutical Formulations
作者： Jéssica S. Stefano , Denise S. Cordeiro , Mariana C. Marra , Eduardo M. Richter , Rodrigo A. A. Munoz
关键词:
摘要: This article highlights the potential use of multi-walled carbon-nanotube modified screen-printed electrodes (SPEs) for amperometric sensing ciprofloxacin and compares association batch-injection analysis (BIA) flow-injection (FIA) with detection. Both analytical systems provided precise (RSD<5 %) sensitive determination (LOD<0.1 μmol L−1) within wide linear range (up to 200 μmol L−1). Accuracy both methods was attested by recovery values (93–107 %) comparison capillary electrophoresis. The BIA system is completely portable (especially due SPEs) faster analyses (130 h−1) more detection than FIA higher flow rates injection.
sci-hub.se 参考文章(44)
E. Bernalte, C. Marín Sánchez, E. Pinilla Gil, High‐Throughput Mercury Monitoring in Indoor Dust Microsamples by Bath Ultrasonic Extraction and Anodic Stripping Voltammetry on Gold Nanoparticles‐Modified Screen‐Printed Electrodes Electroanalysis. ,vol. 25, pp. 289- 294 ,(2013) , 10.1002/ELAN.201200341
Thiago Faria Tormin, Rafael Rodrigues Cunha, Rodrigo Amorim Bezerra da Silva, Rodrigo Alejandro Abarza Munoz, Eduardo Mathias Richter, Combination of screen-printed electrodes and batch injection analysis: A simple, robust, high-throughput, and portable electrochemical system Sensors and Actuators B-chemical. ,vol. 202, pp. 93- 98 ,(2014) , 10.1016/J.SNB.2014.04.096
Katarzyna Michalska, Genowefa Pajchel, Stefan Tyski, Determination of ciprofloxacin and its impurities by capillary zone electrophoresis Journal of Chromatography A. ,vol. 1051, pp. 267- 272 ,(2004) , 10.1016/J.CHROMA.2004.04.048
Fenfen Zhang, Shuqing Gu, Yaping Ding, Zhen Zhang, Li Li, A novel sensor based on electropolymerization of β-cyclodextrin and L-arginine on carbon paste electrode for determination of fluoroquinolones. Analytica Chimica Acta. ,vol. 770, pp. 53- 61 ,(2013) , 10.1016/J.ACA.2013.01.052
Denise Tofanello Gimenes, Polyana Fernandes Pereira, Rafael Rodrigues Cunha, Rodrigo Amorim Bezerra da Silva, Rodrigo Alejandro Abarza Munoz, Eduardo Mathias Richter, A Simple Strategy to Improve the Accuracy of the Injection Step in Batch Injection Analysis Systems with Amperometric Detection Electroanalysis. ,vol. 24, pp. 1805- 1810 ,(2012) , 10.1002/ELAN.201200254
Gustavo Stoppa Garbellini, Romeu C. Rocha-Filho, Orlando Fatibello-Filho, Voltammetric determination of ciprofloxacin in urine samples and its interaction with dsDNA on a cathodically pretreated boron-doped diamond electrode Analytical Methods. ,vol. 7, pp. 3411- 3418 ,(2015) , 10.1039/C5AY00625B
Jonathan P. Metters, Rashid O. Kadara, Craig E. Banks, New directions in screen printed electroanalytical sensors: an overview of recent developments The Analyst. ,vol. 136, pp. 1067- 1076 ,(2011) , 10.1039/C0AN00894J
Xin Zhang, Youli Wei, Yaping Ding, Electrocatalytic oxidation and voltammetric determination of ciprofloxacin employing poly(alizarin red)/graphene composite film in the presence of ascorbic acid, uric acid and dopamine Analytica Chimica Acta. ,vol. 835, pp. 29- 36 ,(2014) , 10.1016/J.ACA.2014.05.020
Margarita Hernández, Carme Aguilar, Francesc Borrull, Marta Calull, Determination of ciprofloxacin, enrofloxacin and flumequine in pig plasma samples by capillary isotachophoresis--capillary zone electrophoresis. Journal of Chromatography B. ,vol. 772, pp. 163- 172 ,(2002) , 10.1016/S1570-0232(02)00071-5
Maria S. M. Quintino, Lúcio Angnes, Batch Injection Analysis: An Almost Unexplored Powerful Tool Electroanalysis. ,vol. 16, pp. 513- 523 ,(2004) , 10.1002/ELAN.200302878