Synthesis of hierarchical copper oxide composites prepared via electrical explosion of the wire in liquids method

作者: Eunju Park , Hyung Wook Park , Jinae Lee

DOI: 10.1016/J.COLSURFA.2015.07.029

关键词:

摘要: Abstract Hierarchical copper oxide particles have attracted recent research interest, due to their structure, properties, and potential applications in catalysis, gas sensing, solar cells, biosensors, lithium ion batteries. In this study, we synthesized hierarchical (CuO/Cu 2 O) structures with various morphologies via electrically induced explosions of Cu wire a liquid. This method does not require surfactant or template can be completed at room temperature. process, particle size shape controlled by varying the energy supplied solution during explosion. Leaf-like, flower-like, rod were generated, composed needle-like building blocks, self-assembly Ostwald ripening. Particle structure morphology investigated using X-ray diffraction, photoelectron spectroscopy, high-resolution transmission electron microscopy, field emission scanning microscopy. The resistance film prepared spin coating was measured. optical band gap determined ultraviolet/visible spectroscopy.

参考文章(37)
Anders Hjelm, Claes G. Granqvist, John M. Wills, Electronic structure and optical properties ofWO3,LiWO3,NaWO3, andHWO3 Physical Review B. ,vol. 54, pp. 2436- 2445 ,(1996) , 10.1103/PHYSREVB.54.2436
Yajuan Mu, Jie Yang, Shuang Han, Hongwei Hou, Yaoting Fan, Syntheses and gas-sensing properties of CuO nanostructures by using [Cu(pbbt)Cl2]2·CH3OH as a precursor Materials Letters. ,vol. 64, pp. 1287- 1290 ,(2010) , 10.1016/J.MATLET.2010.03.010
Shanhu Liu, Ruimin Xing, Feng Lu, Rohit Kumar Rana, Jun-Jie Zhu, One-Pot Template-Free Fabrication of Hollow Magnetite Nanospheres and Their Application as Potential Drug Carriers Journal of Physical Chemistry C. ,vol. 113, pp. 21042- 21047 ,(2009) , 10.1021/JP907296N
Nillohit Mukherjee, Bibhutibhushan Show, Swarup Kumar Maji, Utpal Madhu, Sanjib Kumar Bhar, Bibhas Chandra Mitra, Gobinda Gopal Khan, Anup Mondal, CuO nano-whiskers: Electrodeposition, Raman analysis, photoluminescence study and photocatalytic activity Materials Letters. ,vol. 65, pp. 3248- 3250 ,(2011) , 10.1016/J.MATLET.2011.07.016
Xiaojun Zhang, Dongen Zhang, Xiaomin Ni, Jimei Song, Huagui Zheng, Synthesis and electrochemical properties of different sizes of the CuO particles Journal of Nanoparticle Research. ,vol. 10, pp. 839- 844 ,(2008) , 10.1007/S11051-007-9320-9
A. El-Trass, H. ElShamy, I. El-Mehasseb, M. El-Kemary, CuO nanoparticles: Synthesis, characterization, optical properties and interaction with amino acids Applied Surface Science. ,vol. 258, pp. 2997- 3001 ,(2012) , 10.1016/J.APSUSC.2011.11.025
Haitao Zhu, Jixin Wang, Guiyun Xu, Fast Synthesis of Cu2O Hollow Microspheres and Their Application in DNA Biosensor of Hepatitis B Virus Crystal Growth & Design. ,vol. 9, pp. 633- 638 ,(2009) , 10.1021/CG801006G
Shaodong Sun, Xiaozhe Zhang, Yuexia Sun, Shengchun Yang, Xiaoping Song, Zhimao Yang, None, Hierarchical CuO nanoflowers: water-required synthesis and their application in a nonenzymatic glucose biosensor Physical Chemistry Chemical Physics. ,vol. 15, pp. 10904- 10913 ,(2013) , 10.1039/C3CP50922B