Flow Synthesis of Substituted γ-Lactones by Consecutive Photocatalytic/Reductive Reactions
作者： Maurizio Fagnoni , Filippo Bonassi , Alessandro Palmieri , Stefano Protti , Davide Ravelli
关键词:
摘要: Photolytic addition reaction of aldehydes to activated alkenes and subsequent reduction with hydride under continuous flow conditions provides multisubstituted γ-lactones as mixtures diastereomers.
unicam.it
sci-hub.se 参考文章(69)
Ian R. Baxendale, The integration of flow reactors into synthetic organic chemistry Journal of Chemical Technology & Biotechnology. ,vol. 88, pp. 519- 552 ,(2013) , 10.1002/JCTB.4012
Jun-Ichi Yoshida, Flash chemistry: flow microreactor synthesis based on high‐resolution reaction time control Chemical Record. ,vol. 10, pp. 332- 341 ,(2010) , 10.1002/TCR.201000020
Shinichiro Fuse, Nobutake Tanabe, Masahito Yoshida, Hayato Yoshida, Takayuki Doi, Takashi Takahashi, Continuous-flow synthesis of vitamin D3 Chemical Communications. ,vol. 46, pp. 8722- 8724 ,(2010) , 10.1039/C0CC02239J
M. Teresa Barros, M. Adilia Januario Charmier, Christopher D. Maycock, Thierry Michaud, Synthesis of γ-lactones by desymmetrization. A synthesis of (−)-muricatacin Tetrahedron. ,vol. 65, pp. 396- 399 ,(2009) , 10.1016/J.TET.2008.10.020
Anil Vasudevan, Clara Villamil, Jonathan Trumbull, Jeff Olson, David Sutherland, Jeff Pan, Stevan Djuric, LOPHTOR: a convenient flow-based photochemical reactor Tetrahedron Letters. ,vol. 51, pp. 4007- 4009 ,(2010) , 10.1016/J.TETLET.2010.05.119
George A. Kraus, Peng Liu, Benzophenone-mediated conjugate additions of aromatic aldehydes to quinones Tetrahedron Letters. ,vol. 35, pp. 7723- 7726 ,(1994) , 10.1016/0040-4039(94)80102-9
G. O. Schenck, G. Koltzenburg, H. Grossmann, Durch Benzophenon photosensibilisierte Synthese der Terebinsäure Angewandte Chemie. ,vol. 69, pp. 177- 178 ,(1957) , 10.1002/ANGE.19570690506
Shin Aida, Kimitada Terao, Yasuhiro Nishiyama, Kiyomi Kakiuchi, Michael Oelgemöller, Microflow photochemistry—a reactor comparison study using the photochemical synthesis of terebic acid as a model reaction Tetrahedron Letters. ,vol. 53, pp. 5578- 5581 ,(2012) , 10.1016/J.TETLET.2012.07.143
Brett E. Howard, K.A. Woerpel, Silylene transfer to α-keto esters and application to the synthesis of γ-lactones Tetrahedron. ,vol. 65, pp. 6447- 6453 ,(2009) , 10.1016/J.TET.2009.05.066
Rossella Mello, Andrea Olmos, Javier Parra-Carbonell, María Elena González-Núñez, Gregorio Asensio, Baeyer–Villiger oxidation of ketones with a silica-supported peracid in supercritical carbon dioxide under flow conditions Green Chemistry. ,vol. 11, pp. 994- 999 ,(2009) , 10.1039/B821746G