Prediction of gas chromatographic retention times, column efficiency and resolution as a function of temperature and flow-rate Application for gas chromatographic separation of eight p-hydroxybenzoic esters
作者： Y. Guillaume , M. Thomassin , C. Guinchard
DOI: 10.1016/0021-9673(95)00266-P
关键词:
摘要: Using eight p-hydroxybenzoic esters, simple equations were developed to provide accurate gas chromatographic retention data and column efficiency represented by the height equivalent a theoretical plate. With an experimental design, these have practical applications in calculation of resolution for given pair compounds determination isothermal conditions their separation minimum time. The method reduced number experiments be carried out provided good agreement between results predicted data.
elsevier.com
sci-hub.se 参考文章(30)
Gareth J. Price, Michael R. Dent, Prediction of retention in gas-liquid chromatography using the UNIFAC group contribution method: II. Polymer stationary phases Journal of Chromatography A. ,vol. 585, pp. 83- 92 ,(1991) , 10.1016/0021-9673(91)85060-S
Gareth J. Price, Michael R. Dent, Prediction of retention in gas—liquid chromatography using the unifac group contribution method Journal of Chromatography A. ,vol. 483, pp. 1- 19 ,(1989) , 10.1016/S0021-9673(01)93106-1
E. Fernández-Sánchez, J.A. García-Domínguez, V. Menéndez, J.M. Santiuste, Programmed-temperature retention indices : A survey of calculation methods Journal of Chromatography A. ,vol. 498, pp. 1- 9 ,(1990) , 10.1016/S0021-9673(01)84230-8
J.W. Dolan, L.R. Snyder, D.E. Bautz, Computer simulation as an aid in method development for gas chromatography : II. Changes in band spacing as a function of temperature Journal of Chromatography A. ,vol. 541, pp. 21- 35 ,(1991) , 10.1016/S0021-9673(01)95981-3
C.T. Peng, Z.C. Yang, D. Maltby, Prediction of retention indexes. III. Silylated derivatives of polar compounds. Journal of Chromatography A. ,vol. 586, pp. 113- 129 ,(1991) , 10.1016/0021-9673(91)80029-G
N.W. Davies, Gas chromatographic retention indices of monoterpenes and sesquiterpenes on methyl silicon and Carbowax 20M phases Journal of Chromatography A. ,vol. 503, pp. 1- 24 ,(1990) , 10.1016/S0021-9673(01)81487-4
N. Dimov, E. Matisov'a, Improved method for prediction of gas chromatographic retention indices of C9C12 alkylbenzenes Journal of Chromatography A. ,vol. 549, pp. 325- 333 ,(1991) , 10.1016/S0021-9673(00)91443-2
Tomaso C. Gerbino, Gianrico Castello, Gas chromatographic identification of complex mixtures of halomethanes and haloethanes by using the correlation between their retention and vapour pressure Journal of Chromatography A. ,vol. 537, pp. 305- 319 ,(1991) , 10.1016/S0021-9673(01)88904-4
Andrew D. Jorgensen, Kurt C. Picel, Vassilis C. Stamoudis, Prediction of gas chromatography flame ionization detector response factors from molecular structures Analytical Chemistry. ,vol. 62, pp. 683- 689 ,(1990) , 10.1021/AC00206A007
Louis A. Jones, John J. Glennon, William H. Reis, Critical capillary column examination of the relationship between separation number and height equivalent to a theoretical plate and their dependence on temperature Journal of Chromatography A. ,vol. 595, pp. 209- 219 ,(1992) , 10.1016/0021-9673(92)85164-O