Measurement of screw and edge dislocation density by means of X-ray Bragg profile analysis

作者: E Schafler , M Zehetbauer , T Ungar

DOI: 10.1016/S0921-5093(01)00979-0

关键词:

摘要: Abstract The type of dislocations produced during plastic deformation is necessary to know for the fundamental understanding anisotropy hardening processes. By studying X-ray line broadening in several reflections, fraction certain dislocation types can be determined experimentally. contribution strain generally anisotropic. On basis model, modified Williamson–Hall and Warren–Averbach procedures have been suggested where g g2 are replaced by C , with as average contrast factor. evaluated theoretically different crystal systems types, i.e. edges and/or screws, numerical methods. other hand, analyzing from experiment. Comparing experimental theoretical C-values specific determined. In present paper this procedure has carried out fine grained Cu 99.9% well into stage III. ratio starts a high (90%) screw dislocations. During up e=0.3 picture changes favor edge (75%).

参考文章(19)
T Ungár, A Borbély, None, The effect of dislocation contrast on x‐ray line broadening: A new approach to line profile analysis Applied Physics Letters. ,vol. 69, pp. 3173- 3175 ,(1996) , 10.1063/1.117951
T. Ungar, H. Mughrabi, D. Rönnpagel, M. Wilkens, X-ray line-broadening study of the dislocation cell structure in deformed [001]-orientated copper single crystals Acta Metallurgica. ,vol. 32, pp. 333- 342 ,(1984) , 10.1016/0001-6160(84)90106-8
M Müller, M Zehetbauer, A Borbély, T Ungár, None, Stage IV work hardening in cell forming materials, part I: Features of the dislocation structure determined by X-ray line broadening Scripta Materialia. ,vol. 35, pp. 1461- 1466 ,(1996) , 10.1016/S1359-6462(96)00319-3
T Ungár, I Dragomir, Á Révész, A Borbély, None, The contrast factors of dislocations in cubic crystals: the dislocation model of strain anisotropy in practice Journal of Applied Crystallography. ,vol. 32, pp. 992- 1002 ,(1999) , 10.1107/S0021889899009334
G.K Williamson, W.H Hall, X-ray line broadening from filed aluminium and wolfram Acta Metallurgica. ,vol. 1, pp. 22- 31 ,(1953) , 10.1016/0001-6160(53)90006-6
G. Caglioti, A. Paoletti, F.P. Ricci, Choice of collimators for a crystal spectrometer for neutron diffraction Nuclear Instruments. ,vol. 3, pp. 223- 228 ,(1958) , 10.1016/0369-643X(58)90029-X
Manfred Wilkens, Konrad Eckert, Röntgenographische Untersuchungen über die Versetzungsanordnung in plastisch verformten Kupfer-Einkristallen Zeitschrift für Naturforschung A. ,vol. 19, pp. 459- 470 ,(1964) , 10.1515/ZNA-1964-0410
B.E. Warren, X-ray studies of deformed metals Progress in Metal Physics. ,vol. 8, pp. 147- 202 ,(1959) , 10.1016/0502-8205(59)90015-2