High-resolution 1 H NMR in the solid state using symmetry-based pulse sequences
作者： P.K Madhu , Xin Zhao , Malcolm H Levitt
DOI: 10.1016/S0009-2614(01)00876-4
关键词:
摘要: We demonstrate new rotor synchronised pulse sequences for obtaining high-resolution H-1 NMR spectra in the presence of fast magic angle spinning (MAS). The exploit selection rules generated by appropriate synchronisation radio-frequency (rf) field modulations and sample rotation. show preliminary results demonstrating feasibility proton spectroscopy MAS, also resolution H-1-C-13 J-couplings solid state.
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