A New Bis-amidinium Calix[4]arene-difluorophosphinate Network: An Unexpected but not Unwelcome Guest
作者： Salvatore Camiolo , Philip A. Gale , Mark E. Light , Michael B. Hursthouse
DOI: 10.1080/10610270108039794
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摘要: Abstract A complex hydrogen bonded network is formed between a mono-deprotonated bis-amidinium calix[4]arene 1 and difluorophosphinate in the presence of methanol. The compound crystallises triclinic space group P1 with a=12.0665(5), b=12.5737(6), c=20.0201(15) a, α=86.4098(18), β=79.747(2), γ=66.816(4)°, D c=1.159 Mgm−3 for Z=4.7824 independent reflections were collected final R1 [F 2 > 2α(F 2)] was 0.1243.
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