High-throughput determination of citrinin in rice by ultra-high-performance liquid chromatography and fluorescence detection (UHPLC-FL).
作者： José F. Huertas-Pérez , Natalia Arroyo-Manzanares , Ana M. García-Campaña , Laura Gámiz-Gracia
DOI: 10.1080/19440049.2015.1055522
关键词:
摘要: A rapid, simple and effective method for the determination of citrinin in rice by UHPLC coupled to fluorescence detection has been developed validated. Extraction from samples was achieved applying a QuEChERS-based extraction/partitioning process with water acetonitrile, without need further extract clean-up. The fully validated white rice, its applicability other matrices, such as brown red confirmed recovery experiments. Under optimum conditions, recoveries ranged 72.5% 92.8%, relative standard deviations (RSDs) lower than 7.1%. Detection quantification limits were estimated be 1.5 5.0 µg kg−1, respectively. Finally, 21 organic analysed, but none contaminated above limit method. proved fast non-laborious.
cabdirect.org
sci-hub.se 参考文章(27)
Tseng‐Hsing Wang, Tzann‐Feng Lin, Monascus rice products. Advances in food and nutrition research. ,vol. 53, pp. 123- 159 ,(2007) , 10.1016/S1043-4526(07)53004-4
Youxiang Zhou, Jianbiao Chen, Lina Dong, Liang Lu, Fusheng Chen, Dingjin Hu, Xiaohong Wang, A study of fluorescence properties of citrinin in β-cyclodextrin aqueous solution and different solvents Journal of Luminescence. ,vol. 132, pp. 1437- 1445 ,(2012) , 10.1016/J.JLUMIN.2012.01.005
Natalia Arroyo-Manzanares, José F. Huertas-Pérez, Laura Gámiz-Gracia, Ana M. García-Campaña, A new approach in sample treatment combined with UHPLC-MS/MS for the determination of multiclass mycotoxins in edible nuts and seeds Talanta. ,vol. 115, pp. 61- 67 ,(2013) , 10.1016/J.TALANTA.2013.04.024
L. Pussemier, J.-Y. Piérard, M. Anselme, E. K. Tangni, J.-C. Motte, Y. Larondelle, Development and application of analytical methods for the determination of mycotoxins in organic and conventional wheat. Food Additives and Contaminants Part A-chemistry Analysis Control Exposure & Risk Assessment. ,vol. 23, pp. 1208- 1218 ,(2006) , 10.1080/02652030600699312
T. Sato, K. Higashihara, A. Sasaki, D. Toth, T. Goto, Development and single laboratory validation of a method for citrinin World Mycotoxin Journal. ,vol. 3, pp. 129- 134 ,(2010) , 10.3920/WMJ2010.1204
Ram Y. Gordon, Tod Cooperman, William Obermeyer, David J. Becker, Marked Variability of Monacolin Levels in Commercial Red Yeast Rice Products Buyer Beware JAMA Internal Medicine. ,vol. 170, pp. 1722- 1727 ,(2010) , 10.1001/ARCHINTERNMED.2010.382
Bao-jun Xu, Xiao-qin Jia, Li-juan Gu, Chang-keun Sung, Review on the qualitative and quantitative analysis of the mycotoxin citrinin Food Control. ,vol. 17, pp. 271- 285 ,(2006) , 10.1016/J.FOODCONT.2004.10.012
Katerina Mastovska, Kelly J. Dorweiler, Steven J. Lehotay, Jennifer S. Wegscheid, Kelli A. Szpylka, Pesticide multiresidue analysis in cereal grains using modified QuEChERS method combined with automated direct sample introduction GC-TOFMS and UPLC-MS/MS techniques. Journal of Agricultural and Food Chemistry. ,vol. 58, pp. 5959- 5972 ,(2010) , 10.1021/JF9029892
Natalia Arroyo-Manzanares, José F. Huertas-Pérez, Ana M. García-Campaña, Laura Gámiz-Gracia, Simple methodology for the determination of mycotoxins in pseudocereals, spelt and rice Food Control. ,vol. 36, pp. 94- 101 ,(2014) , 10.1016/J.FOODCONT.2013.07.028
Hongyan Zhang, Mengmeng Wang, Yao Wang, Qingling Li, Jianhua Zhou, Feng Huo, Bo Tang, Preparation and application of an immunoaffinity column based on an antibody with strong affinity and packing material with good stability Food Additives and Contaminants Part A-chemistry Analysis Control Exposure & Risk Assessment. ,vol. 30, pp. 853- 860 ,(2013) , 10.1080/19440049.2013.789932