Determination of Trace Lead Detection in a Sample Solution by Liquid Three-Phase Microextraction–Anodic Stripping Voltammetry
作者： Alireza Allafchian , Seyede Zohreh Mirahmadi-Zare , Marzieh Gholamian
DOI: 10.1109/JSEN.2017.2680450
关键词:
摘要: Herein, the micro extraction and quantification of lead (II) ions were investigated in trace levels on situ pulse anodic stripping voltammetry (DPASV) polytetrafluorethylene (PTFE) membrane-based liquid three-phase extraction. The voltammetric cell contained acceptor solution reference, counter, working electrodes. modified Pt electrode with 3-Trimethoxysilyl-1-propanethiol gold nanoparticles (Au NPs), respectively, was applied as electrode. combined DPASV utilized during time. obtained results showed effect different factors pre-concentration ions, including organic solvent, pH donor phases, concentration complexion agent, time, stirring rate, electrochemical factors; also, optimal conditions established. final stable signal achieved after 18-min time for analytical applications. relative standard deviation enrichment factor to be 6.0% ( $n=5$ ) 18, respectively. calibration curve range 0.207–62.1 ppb Pb(II) (analytical equation: $y=$ 3.986 $x+$ 0.381), limit detection found 0.021 optimum conditions. determined fish, rice, wastewater samples.
harvard.edu
sci-hub.se 参考文章(41)
M. V. Jeevitha, Baby Joseph, Jency George, Impact of heavy metals and Hsp Response International Journal of Biosciences. ,vol. 2, pp. 51- 64 ,(2012)
M. Ghaedi, H. Tavallali, A. Shokrollahi, M. Zahedi, M. Montazerozohori, M. Soylak, Flame atomic absorption spectrometric determination of zinc, nickel, iron and lead in different matrixes after solid phase extraction on sodium dodecyl sulfate (SDS)-coated alumina as their bis (2-hydroxyacetophenone)-1, 3-propanediimine chelates. Journal of Hazardous Materials. ,vol. 166, pp. 1441- 1448 ,(2009) , 10.1016/J.JHAZMAT.2008.12.066
Jing Li, Shaojun Guo, Yueming Zhai, Erkang Wang, High-sensitivity determination of lead and cadmium based on the Nafion-graphene composite film. Analytica Chimica Acta. ,vol. 649, pp. 196- 201 ,(2009) , 10.1016/J.ACA.2009.07.030
Aiguo Lin, Shuai Shao, Huazhou Li, Daoyong Yang, Ying Kong, Preparation and characterization of a new negatively charged polytetrafluoroethylene membrane for treating oilfield wastewater Journal of Membrane Science. ,vol. 371, pp. 286- 292 ,(2011) , 10.1016/J.MEMSCI.2011.01.052
Ali A. Ensafi, B. Saeid, B. Rezaei, Ali R. Allafchian, Differential pulse voltammetric determination of methyldopa using MWCNTs modified glassy carbon decorated with NiFe2O4 nanoparticles Ionics. ,vol. 21, pp. 1435- 1444 ,(2015) , 10.1007/S11581-014-1291-0
Ali A. Ensafi, Ali R. Allafchian, M. Saraji, S. Z. Mirahmadi Zare, Liquid three-phase microextraction based on hollow fiber for highly selective and sensitive determination of desipramine using an ion selective electrode Analytical Methods. ,vol. 3, pp. 463- 470 ,(2011) , 10.1039/C0AY00642D
Guor-Tzo Wei, Zusing Yang, Chao-Jung Chen, Room temperature ionic liquid as a novel medium for liquid/liquid extraction of metal ions Analytica Chimica Acta. ,vol. 488, pp. 183- 192 ,(2003) , 10.1016/S0003-2670(03)00660-3
Ali A. Ensafi, B. Arashpour, B. Rezaei, Ali R. Allafchian, Voltammetric behavior of dopamine at a glassy carbon electrode modified with NiFe2O4 magnetic nanoparticles decorated with multiwall carbon nanotubes Materials Science and Engineering: C. ,vol. 39, pp. 78- 85 ,(2014) , 10.1016/J.MSEC.2014.02.024
T.A. Da Silveira, D.F.D. Araújo, L.C. Marchini, A.C.C.C. Moreti, R.A. Olinda, Detection of metals by differential pulse anodic stripping voltammetry (DPASV) in pollen collected from a fragment of the atlantic forest in Piracicaba/SP Ecotoxicology and Environmental Contamination. ,vol. 8, pp. 31- 36 ,(2013) , 10.5132/EEC.2013.02.005
Serap Seyhan Bozkurt, Sevda Ayata, Ipek Kaynak, Fluorescence-based sensor for Pb(II) using tetra-(3-bromo-4-hydroxyphenyl)porphyrin in liquid and immobilized medium Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. ,vol. 72, pp. 880- 883 ,(2009) , 10.1016/J.SAA.2008.12.012