Growth of glycine ethyl ester hydrochloride and its characterizations
作者： G. Venkatesan , S. Pari
DOI: 10.1016/J.PHYSB.2016.07.038
关键词:
摘要: Abstract Single crystal of glycine ethyl ester hydrochloride by slow evaporation method is reported. The grown characterized single X-ray diffraction, FT-IR, UV–Vis–NIR and fluorescence spectroscopy. It established that the falls under monoclinic system space group P 21/ c with cell parameters as: a =8.565 A, b =12.943 A, =6.272 A, α = γ =90°, β =103.630o. spectrum shows indirect allowed transition band gap 5.21 eV other optical properties are measured. also shown to have high transmittance in visible region. third order nonlinear property limiting been investigated using Z-Scan technique. Complex impedance measured at dc conductivity. Dependence dielectric constant, loss ac conductivity on frequency different temperature applied field analyzed. mechanical behavior has assessed Vickers microhardness indenter. thermal was analyzed TG/DTA curves. From study, material found possess stability up 174 °C. predicted NLO properties, UV–Vis Z-scan studies indicate an attractive for photonics applications.
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iaea.org参考文章(30)
Colin Neville Banwell, Fundamentals of molecular spectroscopy ,(1966)
Peter V.E. McClintock, The origins of life on Earth Contemporary Physics. ,vol. 57, pp. 93- 95 ,(2016) , 10.1080/00107514.2014.999127
S. Natarajan, J. K. Mohana Rao, Crystal structure of bis(glycine)calcium(II)dichloride tetrahydrate Zeitschrift Fur Kristallographie. ,vol. 152, pp. 179- 188 ,(1980) , 10.1524/ZKRI.1980.152.3-4.179
Balvant Shyam Singh, Hyacintha Rennet Lobo, G. Krishna Podagatlapalli, S. Venugopal Rao, Ganapati Subray Shankarling, Thiazole based novel functional colorants: Synthesis, characterization and nonlinear optical studies using picosecond Z-scan technique Optical Materials. ,vol. 35, pp. 962- 967 ,(2013) , 10.1016/J.OPTMAT.2012.11.018
B. R. Lawn, E. R. Fuller, Equilibrium penny-like cracks in indentation fracture Journal of Materials Science. ,vol. 10, pp. 2016- 2024 ,(1975) , 10.1007/BF00557479
D. Bharath, S. Kalainathan, Synthesis, growth, thermal and optical studies on third order nonlinear optical material (E)-2-{3-[2-(4-chlorophenyl) vinyl]-5,5-dimethylcyclo-hex-2-en-1-ylidene}malononitrile for optoelectronic application Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. ,vol. 120, pp. 32- 39 ,(2014) , 10.1016/J.SAA.2013.10.001
K. Boopathi, P. Rajesh, P. Ramasamy, Prapun Manyum, Comparative studies of glycine added potassium dihydrogen phosphate single crystals grown by conventional and Sankaranaryanan-Ramasamy methods Optical Materials. ,vol. 35, pp. 954- 961 ,(2013) , 10.1016/J.OPTMAT.2012.11.015
Mario Rodríguez, Gabriel Ramos-Ortíz, José Luis Maldonado, Victor M Herrera-Ambriz, Oscar Domínguez, Rosa Santillan, Norberto Farfán, Keitaro Nakatani, None, Structural, thermal and optical characterization of a Schiff base as a new organic material for nonlinear optical crystals and films with reversible noncentrosymmetry Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. ,vol. 79, pp. 1757- 1761 ,(2011) , 10.1016/J.SAA.2011.05.051
M. Esthaku Peter, P. Ramasamy, Synthesis, growth and characterization of a novel semiorganic NLO crystal: Triglycine calcium dibromide Journal of Crystal Growth. ,vol. 312, pp. 1952- 1956 ,(2010) , 10.1016/J.JCRYSGRO.2010.03.015
A. Antony Raj, R. Gunaseelan, P. Sagayaraj, Investigation on third order nonlinear optical, electrical and surface properties of organic stilbazolium crystal of 4-N,N-dimethylamino-N′-methylstilbazolium p-methoxybenzenesulfonate Optical Materials. ,vol. 38, pp. 102- 107 ,(2014) , 10.1016/J.OPTMAT.2014.10.011