A FACILE SYNTHESIS OF DIETHYL 1- ISOTHIOCYANO)ALKYLPHOSPHONATES[1]
作者： D. Sikora , T. Gajda
DOI: 10.1080/10426500008040523
关键词:
摘要: Abstract Novel, diethyl 1-(isothiocyano)alkylphosphonates 3 have been efficiently synthesized via a one-pot reaction of 1-azidoalkylphosphonates 1 with triphenylphosphine, followed by in situ transformation thus formed phosphazenes 2 carbon disulfide. Application the title compounds synthesis (N-phenylthioureido)- and (benzothiazol-2-ylamino)methylphosphonates was also described.
sci-hub.se 参考文章(13)
. Drobnica, P. Kristin, J. Augustn, The chemistry of the — NCS group John Wiley & Sons, Ltd. pp. 1003- 1221 ,(2010) , 10.1002/9780470771532.CH6
Alan R. Katritzky, Jinlong Jiang, John V. Greenhill, 1,2- and 1,3-Monoazabisylides as novel synthons Journal of Organic Chemistry. ,vol. 58, pp. 1987- 1988 ,(1993) , 10.1021/JO00060A002
D.J. Harvey, M.G. Horning, Derivatives for the characterization of alkyl- and aminoalkylphosphonates by gas chromatography and gas chromatography-mass spectrometry Journal of Chromatography A. ,vol. 79, pp. 65- 74 ,(1973) , 10.1016/S0021-9673(01)85274-2
Satyavan Sharma, Isothiocyanates in Heterocyclic Synthesis Sulfur Reports. ,vol. 8, pp. 327- 454 ,(1989) , 10.1080/01961778908046181
Arya K. Mukerjee, Ram. Ashare, Isothiocyanates in the chemistry of heterocycles Chemical Reviews. ,vol. 91, pp. 1- 24 ,(1991) , 10.1021/CR00001A001
H. Staudinger, Ernst Hauser, Über neue organische Phosphorverbindungen IV Phosphinimine Helvetica Chimica Acta. ,vol. 4, pp. 861- 886 ,(1921) , 10.1002/HLCA.19210040192
D. J. Harvey, M. G. Horning, The mass spectra of the trimethylsilyl esters of acetyl, schiff base and isothiocyanate derivatives of some aminoalkylphosphonic acids Journal of Mass Spectrometry. ,vol. 9, pp. 955- 969 ,(1974) , 10.1002/OMS.1210091002
Narahari Babu Ambati, V. Anand, P. Hanumanthu, A Facile Synthesis of 2-N(Methyl Amino) Benzothiazoles Synthetic Communications. ,vol. 27, pp. 1487- 1493 ,(1997) , 10.1080/00397919708006084
Dorota Sikora, Tadeusz Gajda, A CONVENIENT SYNTHESIS OF 5-SUBSTITUTED 1-1-(DIETHOXYPHOSPHORYL)ALKYL-1H-1,2,3-TRIAZOLES Synthetic Communications. ,vol. 28, pp. 1215- 1222 ,(1998) , 10.1080/00397919808005963
S Andronati, O.V. Kobzareva, A.V. Bogatskii, Z.I. Zhilina, T.K. Chumachenko, R Ivanova, P.A. Sharbatyan, Zh. Obshch. Khim. ,(1975)