Modernization and validation of an isoperibol rotating bomb calorimeter for the measurement of energies of combustion of sulphur compounds

作者: Mohammed Ellaite , Didier Dalmazzone

DOI: 10.1007/S10973-009-0555-9

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摘要: A rotating bomb calorimeter belonging to the Laboratory of Chemistry and Process Engineering (UCP) at ENSTA ParisTech since 1960s was modernized re-set in order service for measurement heats combustion sulphur-containing compounds. The parts that were replaced concerned essentially thermal regulation, firing system data acquisition, while most mechanical organs found work perfectly. apparatus tested extensively calibrated using standard benzoic acid. energy thianthrene measured validate operating protocol sulphur

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