Cyclodextrin polymer/Fe3O4 nanocomposites as solid phase extraction material coupled with UV-vis spectrometry for the analysis of rutin.
作者： Aiqin Gong , Wenhui Ping , Jue Wang , Xiashi Zhu
DOI: 10.1016/J.SAA.2013.11.050
关键词:
摘要: Abstract In this paper, carboxymethyl-hydroxypropyl-β-cyclodextrin polymer modified magnetic particles Fe3O4 (CM-HP-β-CDCP-MNPs) were prepared and applied to solid phase extraction of rutin combined with UV–visible spectrometry detection. The synthesized characterized by element analysis, Fourier transform infrared spectra, thermal gravimetric transmission electron microscopy. Several variables affecting the desorption such as pH, amount adsorbent, type volume eluent, time, temperature investigated. maximum adsorption capacity was 67.0 mg g−1 for equilibrium time 30 min at room temperature, adsorbent could be reused 10 times. A calibration curve linear in range 0.05–8.00 μg mL−1 a relative standard deviation 2.9% (n = 5, c = 4.0 μg mL−1). limit detection 7.0 ng mL−1. interaction mechanism between also studied. Feasibility method validated analysis tablets lotus plumule.
harvard.edu
sci-hub.se 参考文章(25)
Luís Mafra, José Alejandro Vidal-Moya, Teresa Blasco, Structural Characterization of Zeolites by Advanced Solid State NMR Spectroscopic Methods Annual Reports on NMR Spectroscopy. ,vol. 77, pp. 259- 351 ,(2012) , 10.1016/B978-0-12-397020-6.00004-0
Hongwei Wu, Meilan Chen, Yunchang Fan, Fawzi Elsebaei, Yan Zhu, Determination of rutin and quercetin in Chinese herbal medicine by ionic liquid-based pressurized liquid extraction-liquid chromatography-chemiluminescence detection. Talanta. ,vol. 88, pp. 222- 229 ,(2012) , 10.1016/J.TALANTA.2011.10.036
A.Z.M. Badruddoza, Goh Si Si Hazel, K. Hidajat, M.S. Uddin, Synthesis of carboxymethyl-β-cyclodextrin conjugated magnetic nano-adsorbent for removal of methylene blue Colloids and Surfaces A: Physicochemical and Engineering Aspects. ,vol. 367, pp. 85- 95 ,(2010) , 10.1016/J.COLSURFA.2010.06.018
H. Abdolmohammad-Zadeh, Z. Rezvani, G.H. Sadeghi, E. Zorufi, Layered double hydroxides: a novel nano-sorbent for solid-phase extraction. Analytica Chimica Acta. ,vol. 685, pp. 212- 219 ,(2011) , 10.1016/J.ACA.2010.11.035
Marija Vukcevic, Ana Kalijadis, Marina Radisic, Biljana Pejic, Mirjana Kostic, Zoran Lausevic, Mila Lausevic, Application of carbonized hemp fibers as a new solid-phase extraction sorbent for analysis of pesticides in water samples Chemical Engineering Journal. ,vol. 211-212, pp. 224- 232 ,(2012) , 10.1016/J.CEJ.2012.09.059
J. Wang, H. Wang, S. Han, Ultrasensitive determination of epicatechin, rutin, and quercetin by capillary electrophoresis chemiluminescence Acta Chromatographica. ,vol. 24, pp. 679- 688 ,(2012) , 10.1556/ACHROM.24.2012.4.13
Dalia Panavaitė, Audrius Padarauskas, Vida Vičkačkaitė, Silicone glue coated stainless steel wire for solid phase microextraction. Analytica Chimica Acta. ,vol. 571, pp. 45- 50 ,(2006) , 10.1016/J.ACA.2006.04.035
Lin Peng, Yuzhi Wang, Huan Zeng, Ya Yuan, Molecularly imprinted polymer for solid-phase extraction of rutin in complicated traditional Chinese medicines The Analyst. ,vol. 136, pp. 756- 763 ,(2011) , 10.1039/C0AN00798F
Abu Zayed M. Badruddoza, Zayed Bin Zakir Shawon, Wei Jin Daniel Tay, Kus Hidajat, Mohammad Shahab Uddin, Fe3O4/cyclodextrin polymer nanocomposites for selective heavy metals removal from industrial wastewater. Carbohydrate Polymers. ,vol. 91, pp. 322- 332 ,(2013) , 10.1016/J.CARBPOL.2012.08.030
Yinshi Sun, Wei Li, Jianhua Wang, Jianjie Bi, Shudong Su, Determination of rutin in cigarette tobacco, filters, mainstream smoke and burned ash of different branded cigarettes by high performance liquid chromatography. Molecules. ,vol. 17, pp. 3751- 3760 ,(2012) , 10.3390/MOLECULES17043751