Synthesis and Crystal Structure of Tridodecylammonium 3,5-Dinitro-1, 2, 4-1H-triazolate (TDADNT)

作者: Tao Zhang , Long Liu , Yan Qiang Zhang , Zeng Xi Li

DOI: 10.4028/WWW.SCIENTIFIC.NET/AMR.881-883.205

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摘要: Tridodecylammonium 3,5-dinitro-1,2,4-1H-triazolate (TDADNT) was synthesized and characterized by NMR, IR, Raman spectra, elemental analysis TG/DTA. Its structure further confirmed the single crystal X-ray diffraction (Fig. 2), which shows that compound crystallizes in triclinic space group P-1 with a = 8.9507(19) A, b 12.702(2) c 19.068(4) α 72.440(5) o, β 89.620(7) γ 84.901(7) V 2058.3(7) A3, Z 2. The salt is thermally stable up to 270 °C TG/DTA measurements.

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