DETERMINATION OF SILICATE ANIONS BY GAS CHROMATOGRAPHIC SEPARATION AND MASS SPECTROMETRIC IDENTIFICATION OF THEIR TRIMETHYLSILYL DERIVATIVES
作者： F.F.H. Wu , J. Götz , W.D. Jamieson , C.R. Masson
DOI: 10.1016/S0021-9673(01)85585-0
关键词:
摘要: The trimethylsilyl derivatives of the anions SiO44−, Si2O76−, Si3O96−, Si3O108− and Si4O128− were resolved below 290° on SE-30 (methylpolysiloxane) liquid phase using a temperature-programmed operation identified by high-resolution mass spectrometry. cracking pattern these in spectrometer is discussed.
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sci-hub.se 参考文章(4)
Charles W. Lentz, Silicate Minerals as Sources of Trimethylsilyl Silicates and Silicate Structure Analysis of Sodium Silicate Solutions Inorganic Chemistry. ,vol. 3, pp. 574- 579 ,(1964) , 10.1021/IC50014A029
Don C. DeJongh, T. Radford, Jeremy D. Hribar, Stephen Hanessian, M. Bieber, G. Dawson, C. C. Sweeley, Analysis of trimethylsilyl derivatives of carbohydrates by gas chromatography and mass spectrometry Journal of the American Chemical Society. ,vol. 91, pp. 1728- 1740 ,(1969) , 10.1021/JA01035A022
W. Wieker, D. Hoebbel, Chemische Untersuchungen von Silicaten. - XXXVI : Die papierchromatographische Untersuchung von kondensierten Silicaten und Kieselsäuren Zeitschrift für anorganische und allgemeine Chemie. ,vol. 366, pp. 139- 151 ,(1969) , 10.1002/ZAAC.19693660305
K. M. Baker, M. A. Shaw, Dudley H. Williams, Mass spectra of trimethylsilyl derivatives of some amino-acids and peptides Journal of the Chemical Society D: Chemical Communications. pp. 1108- 1109 ,(1969) , 10.1039/C29690001108