Synthesis and characterization of a new nano lead(II) 0-D coordination supramolecular compound: A precursor to produce pure phase nano-sized lead(II) oxide.
作者： Mohammad Jaafar Soltanian Fard , Payam Hayati , Hakimeh Sadat Naraghi , Sayed Abbas Tabeie
DOI: 10.1016/J.ULTSONCH.2017.04.023
关键词:
摘要: Nano-structure of a new 0D Pb(II) coordination supramolecular compound, [Pb4(8-Quin)6](ClO4)2(1), L=8-HQuin=8-hydroxyquinolin ligand has been synthesized by use sonochemical process and characterized scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infrared spectroscopy (FTIR) elemental analyses. The structure compound 1 was determined single-crystal diffraction. single crystal data implies that the Pb+2 ions are five coordinated. Each lead atom is coordinated to nitrogen oxygen atoms 8-hydroxyquinolin ligand. Topological analysis shows 1,2,3,4,4M12-1net. Nanoparticles lead(II) oxide have prepared calcination polymer at 500°C were (XRPD) IR spectroscopy.
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