Structural Characterization of Micromechanical Properties in Asphalt Using Atomic Force Microscopy

作者: R. Grover Allen , Dallas N. Little , Amit Bhasin

DOI: 10.1061/(ASCE)MT.1943-5533.0000510

关键词:

摘要: This paper semiquantitatively evaluates the microrheological properties of asphalt binder using atomic force microscopy. It also presents differences between these amongst various microstructures within an binder, in addition to influence oxidative aging on properties. Nano-indentation experiments performed a microgrid phases determined micromechanical such as stiffness, adhesion, and elastic/plastic behavior. The evaluated materials include asphalts AAB, AAD, ABD from Materials Reference Library Strategic Highway Research Program, chosen because variations crude source, chemical composition, elemental analysis. Analysis nano-indentation creep measurements corresponding phase-separated regions revealed heterogeneous domains with different mechanical properties, induced substantial microstructural change domains, including phase structure, distribution. form extent changes, however, were for each asphalt. Interpretation data collected microcopy this study advances understanding composition binders response under load, how responses aging.

参考文章(23)
J S Moulthrop, M Mortazavi, THE SHRP MATERIALS REFERENCE LIBRARY ,(1993)
R Robert, Troy Pauli, Nicole Kringos, A Thermodynamical Approach to Healing in Bitumen 7th RILEM Conference on Advanced Testing and Characterization of Bituminous Materials. Rhodes, Greece. 27-29 May 2009. ,(2009)
D R Jones, T W Kennedy, THE ASPHALT MODEL: RESULTS OF THE SHRP ASPHALT RESEARCH PROGRAM Proceedings of the Conference, Strategic Highway Research Program and Traffic Safety on Two Continents, Part Four. ,(1991)
Nancy A. Burnham, Dawn D. Dominguez, Robert L. Mowery, Richard J. Colton, Probing the surface forces of monolayer films with an atomic-force microscope. Physical Review Letters. ,vol. 64, pp. 1931- 1934 ,(1990) , 10.1103/PHYSREVLETT.64.1931
S-C Huang, TF Turner, AT Pauli, FP Miknis, JF Branthaver, RE Robertson, Evaluation of Different Techniques for Adhesive Properties of Asphalt-Filler Systems at Interfacial Region Journal of Astm International. ,vol. 2, pp. 1- 15 ,(2005) , 10.1520/JAI12961
J-F. MASSON, V. LEBLOND, J. MARGESON, Bitumen morphologies by phase-detection atomic force microscopy. Journal of Microscopy. ,vol. 221, pp. 17- 29 ,(2006) , 10.1111/J.1365-2818.2006.01540.X
Andreas Jäger, Roman Lackner, Klaus Stangl, Microscale characterization of bitumen – back-analysis of viscoelastic properties by means of nanoindentation International Journal of Materials Research. ,vol. 98, pp. 404- 413 ,(2007) , 10.3139/146.101486
J. Ph. Pfeiffer, R. N. J. Saal, Asphaltic Bitumen as Colloid System. The Journal of Physical Chemistry. ,vol. 44, pp. 139- 149 ,(1940) , 10.1021/J150398A001
L. LOEBER, O. SUTTON, J. MOREL, J.-M. VALLETON, G. MULLER, NEW DIRECT OBSERVATIONS OF ASPHALTS AND ASPHALT BINDERS BY SCANNING ELECTRON MICROSCOPY AND ATOMIC FORCE MICROSCOPY Journal of Microscopy. ,vol. 182, pp. 32- 39 ,(1996) , 10.1046/J.1365-2818.1996.134416.X