Structural biology applications of solid state MAS DNP NMR.
作者： Ümit Akbey , Hartmut Oschkinat
DOI: 10.1016/J.JMR.2016.04.003
关键词:
摘要: Dynamic Nuclear Polarization (DNP) has long been an aim for increasing sensitivity of nuclear magnetic resonance (NMR) spectroscopy, delivering spectra in shorter experiment times or smaller sample amounts. In recent years, it applied magic angle spinning (MAS) solid-state NMR to a large range samples, including biological macromolecules and functional materials. New research directions structural biology can be envisaged by DNP, facilitating investigations on very complexes heterogeneous samples. Here we present summary state the art DNP MAS spectroscopy its applications biology, discussing technical challenges factors affecting performance.
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