Structure and Phase Transition of 4,7-Bis-(4′-cyano-biphenyl-4-yl)-[1, 10]phenanthroline
作者： Brenden Carlson , Werner Kaminsky , Linyue Tong , Gregory D. Phelan
DOI: 10.1007/S10870-015-0614-Y
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摘要: Bis-(4′-cyano-biphenyl-4-yl)-[1, 10] phenanthroline (cnbiphphen) is synthesized from a palladium mediated coupling between 4-cyanobenzene boronic acid and 4, 7-bis (4-bromophenyl)-[1, 10] phenanthroline. The single crystal X-ray structure was measured at both 298 (2) K and 90 (2) K. The asymmetric unit of the title compound in the low-temperature phase, C 38 H 22 N 4. HCCl 3, is comprised of one cnbiphphen molecule and one chloroform solvent molecule. Additional symmetry relates one-half of the title compound …
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sci-hub.se 参考文章(28)
Angela Altomare, Maria Cristina Burla, Mercedes Camalli, Giovanni Luca Cascarano, Carmelo Giacovazzo, Antonietta Guagliardi, Anna Grazia Giuseppina Moliterni, Giampiero Polidori, Riccardo Spagna, SIR97: a new tool for crystal structure determination and refinement Journal of Applied Crystallography. ,vol. 32, pp. 115- 119 ,(1999) , 10.1107/S0021889898007717
A. Juris, V. Balzani, F. Barigelletti, S. Campagna, P. Belser, A. von Zelewsky, Ru(II) polypyridine complexes: photophysics, photochemistry, eletrochemistry, and chemiluminescence Coordination Chemistry Reviews. ,vol. 84, pp. 85- 277 ,(1988) , 10.1016/0010-8545(88)80032-8
Elisabeth Gerber, Anne Bredy, Regine Kahl, Ortho-phenanthroline modulates enzymes of cellular energy metabolism☆ Toxicology. ,vol. 110, pp. 85- 93 ,(1996) , 10.1016/0300-483X(96)03331-8
Stephan Foerster, Ashish K. Khandpur, Jin Zhao, Frank S. Bates, Ian W. Hamley, Anthony J. Ryan, Wim Bras, Complex Phase Behavior of Polyisoprene-Polystyrene Diblock Copolymers Near the Order-Disorder Transition Macromolecules. ,vol. 27, pp. 6922- 6935 ,(1994) , 10.1021/MA00101A033
T. Besara, P. Jain, N. S. Dalal, P. L. Kuhns, A. P. Reyes, H. W. Kroto, A. K. Cheetham, Mechanism of the order–disorder phase transition, and glassy behavior in the metal-organic framework [(CH3)2NH2]Zn(HCOO)3 Proceedings of the National Academy of Sciences of the United States of America. ,vol. 108, pp. 6828- 6832 ,(2011) , 10.1073/PNAS.1102079108
Jaana Tammiku, Peeter Burk, Ants Tuulmets, 1,10-Phenanthroline and Its Complexes with Magnesium Compounds. Disproportionation Equilibria Journal of Physical Chemistry A. ,vol. 105, pp. 8554- 8561 ,(2001) , 10.1021/JP011476N
Miso Jeong, Hyungoog Nam, Ok-Jae Sohn, Jong Il Rhee, Hyung Jin Kim, Chang-Woo Cho, Sunwoo Lee, Synthesis of phenanthroline derivatives by Sonogashira reaction and the use of their ruthenium complexes as optical sensors Inorganic Chemistry Communications. ,vol. 11, pp. 97- 100 ,(2008) , 10.1016/J.INOCHE.2007.11.001
Francis H. Case, Substituted 1,10-Phenanthrolines. V. Phenyl Derivatives Journal of Organic Chemistry. ,vol. 16, pp. 1541- 1545 ,(1951) , 10.1021/JO50004A008
H. J. Coles, C. Strazielle, The Order-Disorder Phase Transition in Liquid Crystals as a Function of Molecular Structure. I. The Alkyl Cyanobiphenyls Molecular Crystals and Liquid Crystals. ,vol. 55, pp. 237- 250 ,(1979) , 10.1080/00268947908069805
Peter C. Alford, Michael J. Cook, Anthony P. Lewis, Glenn S. G. McAuliffe, Vladimir Skarda, Andrew J. Thomson, John L. Glasper, David J. Robbins, Luminescent metal complexes. Part 5. Luminescence properties of ring-substituted 1,10-phenanthroline tris-complexes of ruthenium(II) Journal of The Chemical Society-perkin Transactions 1. ,vol. 16, pp. 705- 709 ,(1985) , 10.1039/P29850000705