A Convenient Void Volume Marker for Several Chiral HPLC Columns
作者： William H. Pirkle , Christopher J. Welch
DOI: 10.1080/01483919108049593
关键词:
摘要: Abstract Comparison of a number potential void volume markers under normal phase conditions shows 1,3,5-Tri-t-butylbenzene (TTBB) to be essentially unretained on three commercially available chiral stationary phases (CSPs). Elution times observed for TTBB agree well with determined by the method minor disturbance, or pycnometrically total mobile (Vm). Therefore is recommended use as marker separations these CSPs.
sci-hub.se 参考文章(20)
Roelof F. Rekker, Gerrit De Vries, Greetje J. Bijloo, Retention studies of alkyl- and halogen-substituted aromatics on normal-phase silica and alumina columns Journal of Chromatography A. ,vol. 370, pp. 355- 376 ,(1986) , 10.1016/S0021-9673(00)94709-5
Helmut Koller, Karl-Heinz Rimböck, Albrecht Mannschreck, High-pressure liquid chromatography on triacetylcellulose Journal of Chromatography A. ,vol. 282, pp. 89- 94 ,(1983) , 10.1016/S0021-9673(00)91594-2
Franco Pasutto, Chiral Separations by HPLC: Applications to Pharmaceutical Compounds. Journal of Pharmaceutical Sciences. ,vol. 79, pp. 1043- 1044 ,(1990) , 10.1002/JPS.2600791124
E.H. Slaats, J.C. Kraak, W.J.T. Brugman, H. Poppe, Study of the influence of competition and solvent interaction on retention in liquid-solid chromatography by measurement of activity coefficients in the mobile phase Journal of Chromatography A. ,vol. 149, pp. 255- 270 ,(1978) , 10.1016/S0021-9673(00)80991-7
R. A. Djerki, R. J. Laub, Solute retention in column liquid chromatography. XI. Exposition of the minor-disturbance method of measurement of the void volume Journal of Liquid Chromatography & Related Technologies. ,vol. 11, pp. 327- 332 ,(1988) , 10.1080/01483918809349943
J. N. Akanya, D. R. Taylor, The effect of temperature on the resolution of racemates on a chiral bonded packing incorporating N-formylphenylalanine Chromatographia. ,vol. 25, pp. 639- 642 ,(1988) , 10.1007/BF02327663
R.P.W. Scott, P. Kucera, The exclusion properties of some commercially available silica gels Journal of Chromatography A. ,vol. 125, pp. 251- 263 ,(1976) , 10.1016/S0021-9673(00)93823-8
Christine E. Evans, John G. Shabushing, Victoria L. McGuffin, Experimental and theoretical model of refractive index artifacts in absorbance detection Journal of Chromatography A. ,vol. 459, pp. 119- 138 ,(1988) , 10.1016/S0021-9673(01)82021-5
William H. Pirkle, James L. Schreiner, Chiral HPLC (high-performance liquid chromatographic) stationary phases. 4. Separation of the enantiomers of bi-.beta. naphthols and analogs Journal of Organic Chemistry. ,vol. 13, pp. 4988- 4991 ,(1981) , 10.1021/JO00337A033
R. J. Smith, C. S. Nieass, M. S. Wainwright, A review of methods for the determination of hold-up volume in modern liquid chromatography Journal of Liquid Chromatography & Related Technologies. ,vol. 9, pp. 1387- 1430 ,(1986) , 10.1080/01483918608076694