Synthesis of cyclic phenyl hexayne from Me3Si-/Ph2P(O)-protected ethynes:

作者: Li Wu , Li-fen Peng , Zhi-fang Hu , Hong Wang , Zi-long Tang

DOI: 10.1177/1747519819874419

关键词:

摘要: A practical approach for the synthesis of cyclic phenyl hexayne is demonstrated through a one-pot deprotection/transformation magnesium acetylide into copper acetylide/Sonogashira coupling pro...

参考文章(24)
Lifen Peng, Feng Xu, Kenta Shinohara, Akihiro Orita, Junzo Otera, Selective Deprotection of Me3Si-/Ph2P(O)-protected Arylalkynes: Methyl Grignard Reagent-promoted Dephosphorylation of Ph2P(O)-protected Alkynes Chemistry Letters. ,vol. 43, pp. 1610- 1612 ,(2014) , 10.1246/CL.140579
Lifen Peng, Feng Xu, Yoshinori Suzuma, Akihiro Orita, Junzo Otera, One-Pot Transformation of Ph2P(O)-Protected Ethynes: Deprotection Followed by Transition Metal-Catalyzed Coupling Journal of Organic Chemistry. ,vol. 78, pp. 12802- 12808 ,(2013) , 10.1021/JO402176W
Matthias Fischer, Günter Lieser, Almut Rapp, Ingo Schnell, Wael Mamdouh, Steven De Feyter, Frans C. De Schryver, Sigurd Höger, Shape-persistent macrocycles with intraannular polar groups: synthesis, liquid crystallinity, and 2D organization. Journal of the American Chemical Society. ,vol. 126, pp. 214- 222 ,(2004) , 10.1021/JA038484X
Rafael Chinchilla, Carmen Nájera, The Sonogashira Reaction: A Booming Methodology in Synthetic Organic Chemistry† Chemical Reviews. ,vol. 107, pp. 874- 922 ,(2007) , 10.1021/CR050992X
Xin Yang, Shingo Kajiyama, Jing-Kun Fang, Feng Xu, Yu Uemura, Nagatoshi Koumura, Kohjiro Hara, Akihiro Orita, Junzo Otera, Synthesis and Properties of Anthrylene-Substituted Phenyleneethynylene Dyes Having Amino/Cyano Group(s) and Their Application to Dye-Sensitized Solar Cells Bulletin of the Chemical Society of Japan. ,vol. 85, pp. 687- 697 ,(2012) , 10.1246/BCSJ.20110390
Takahito Oyamada, Guang Shao, Hiroyuki Uchiuzou, Hajime Nakanotani, Akihiro Orita, Junzo Otera, Masayuki Yahiro, Chihaya Adachi, Optical and Electrical Properties of Bis(4-(phenylethynyl)phenyl)ethynes and Their Application to Organic Field-Effect Transistors Japanese Journal of Applied Physics. ,vol. 45, pp. L1331- L1333 ,(2006) , 10.1143/JJAP.45.L1331
Chao Wu, Panpan Yang, Zhimin Fu, Yong Peng, Xin Wang, Zuozhi Zhang, Fang Liu, Wenyi Li, Zhizhang Li, Weimin He, Regio- and Stereoselective Hydrosulfonation of Alkynylcarbonyl Compounds with Sulfinic Acid in Water. Journal of Organic Chemistry. ,vol. 81, pp. 10664- 10671 ,(2016) , 10.1021/ACS.JOC.6B01549
Chao Wu, Xiu Xin, Zhi-Min Fu, Long-Yong Xie, Kai-Jian Liu, Zheng Wang, Wenyi Li, Zhi-Hui Yuan, Wei-Min He, Water-controlled selective preparation of α-mono or α,α′-dihalo ketones via catalytic cascade reaction of unactivated alkynes with 1,3-dihalo-5,5-dimethylhydantoin Green Chemistry. ,vol. 19, pp. 1983- 1989 ,(2017) , 10.1039/C7GC00283A
Lifen Peng, Rongzhen Li, Zilong Tang, Jingyang Chen, Rongnan Yi, Xinhua Xu, Cesium-catalyzed highly regioselective synthesis of (Z)-vinylic selenosulfides via thioselenation of alkynes with unsymmetrical diorganoyl dichalcogenides Tetrahedron. ,vol. 73, pp. 3099- 3105 ,(2017) , 10.1016/J.TET.2017.04.009
Chao Wu, Zheng Wang, Zhan Hu, Fei Zeng, Xing-Yu Zhang, Zhong Cao, Zilong Tang, Wei-Min He, Xin-Hua Xu, Direct synthesis of alkenyl iodides via indium-catalyzed iodoalkylation of alkynes with alcohols and aqueous HI Organic and Biomolecular Chemistry. ,vol. 16, pp. 3177- 3180 ,(2018) , 10.1039/C8OB00183A