Correlation of stress and texture evolution during self- and thermal annealing of electroplated Cu films

作者: Haebum Lee , S. Simon Wong , Sergey D. Lopatin

DOI: 10.1063/1.1555274

关键词:

摘要: Electroplated Cu films with different plating conditions and thicknesses are characterized to study the stress texture evolution involved in transition of microstructure during self-annealing. Grain growth process induces film tensile direction. Degradation (111) enhancement (200) observed microstructural transition. The rate self-annealing increases dramatically as current density increases. Self-annealing is significantly retarded thinner plated pulse reverse current. A strong correlation between development demonstrated for all electroplated under self- thermal annealing conditions. This explained by surface/interface energy strain anisotropic metal films. Due mechanical anisotropy Cu, orientation lowest total changes from dominant ...

参考文章(17)
S. Vaidya, A.K. Sinha, Effect of texture and grain structure on electromigration in Al-0.5%Cu thin films Thin Solid Films. ,vol. 75, pp. 253- 259 ,(1981) , 10.1016/0040-6090(81)90404-1
Kazuyoshi Ueno, Tom Ritzdorf, Scott Grace, Seed layer dependence of room-temperature recrystallization in electroplated copper films Journal of Applied Physics. ,vol. 86, pp. 4930- 4935 ,(1999) , 10.1063/1.371462
S. K. Jung, S. W. Hwang, J. H. Park, B. D. Min, E. K. Kim, Yong Kim, Lateral Transport through Self-Assembled InAs Quantum Dots Located in the Narrow Gap Electrodes MRS Proceedings. ,vol. 571, pp. 209- 213 ,(1999) , 10.1557/PROC-571-209
C. Lingk, M. E. Gross, RECRYSTALLIZATION KINETICS OF ELECTROPLATED CU IN DAMASCENE TRENCHES AT ROOM TEMPERATURE Journal of Applied Physics. ,vol. 84, pp. 5547- 5553 ,(1998) , 10.1063/1.368856
C.V. Thompson, Texture evolution during grain growth in polycrystalline films Scripta Metallurgica et Materialia. ,vol. 28, pp. 167- 172 ,(1993) , 10.1016/0956-716X(93)90557-9
D. B. Knorr, D. P. Tracy, K. P. Rodbell, Correlation of texture with electromigration behavior in Al metallization Applied Physics Letters. ,vol. 59, pp. 3241- 3243 ,(1991) , 10.1063/1.105745
D. P. Tracy, D. B. Knorr, Texture and microstructure of thin copper films Journal of Electronic Materials. ,vol. 22, pp. 611- 616 ,(1993) , 10.1007/BF02666406
D. P. Tracy, D. B. Knorr, K. P. Rodbell, Texture in multilayer metallization structures Journal of Applied Physics. ,vol. 76, pp. 2671- 2680 ,(1994) , 10.1063/1.357564
W.W Mullins, The effect of thermal grooving on grain boundary motion Acta Metallurgica. ,vol. 6, pp. 414- 427 ,(1958) , 10.1016/0001-6160(58)90020-8
JME Harper, C Cabral Jr, PC Andricacos, L Gignac, IC Noyan, KP Rodbell, CK Hu, None, Mechanisms for microstructure evolution in electroplated copper thin films near room temperature Journal of Applied Physics. ,vol. 86, pp. 2516- 2525 ,(1999) , 10.1063/1.371086