A Practical Method for the Large-Scale Preparation of [N,N'-Bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]manganese(III) chloride, a Highly Enantioselective Epoxidation Catalyst

作者: Jay F. Larrow , Eric N. Jacobsen , Yun Gao , Yaping Hong , Xiaoyi Nie

DOI: 10.1021/JO00086A062

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摘要: … 1 h and the precipitated brown solid was collected by vacuum filtration. The catalyst was dried under high vacuum at 50-60 eC for 12 h … 580" (c 0.01, EtOH); IR (KBr) v 2958-2950, 2912,…

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