Verification of the findings of acrylamide in heated foods.

作者: J. S. Ahn , L. Castle , D. B. Clarke , A. S. Lloyd , M. R. Philo

DOI: 10.1080/0265203021000048214

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摘要: We report here the first confirmation of recent Swedish findings acrylamide in heated foods. The verification exercise used an LC-MS/MS method developed for purpose as well established GCMS analysis. was suitable direct determination aqueous extracts foods by isotope dilution mass spectrometry (IDMS) using triply deuterated acrylamide. Some food matrices were not suited to new and mixed-mode solid-phase extraction (SPE) clean these extracts. tested included UK versions some key groups analysed Sweden. Also under home-cooking conditions. There good agreement between results GC-MS levels found similar those reported corresponding study. analyses confirmed that is absent from raw or boiled but present at significant fried, grilled, baked toasted highest result 12000 microg kg(-1) overcooked oil-fried chips.

参考文章(7)
C. Brede, I. Skjevrak, H. Herikstad, E. Ånensen, R. Austvoll, T. Hemmingsen, Improved sample extraction and clean-up for the GC-MS determination of BADGE and BFDGE in vegetable oil. Food Additives and Contaminants Part A-chemistry Analysis Control Exposure & Risk Assessment. ,vol. 19, pp. 483- 491 ,(2002) , 10.1080/02652030110088293
Johan Rosén, Karl-Erik Hellenäs, Analysis of acrylamide in cooked foods by liquid chromatography tandem mass spectrometry. Analyst. ,vol. 127, pp. 880- 882 ,(2002) , 10.1039/B204938D
Eden Tareke, Per Rydberg, Patrik Karlsson, Sune Eriksson, Margareta Törnqvist, Analysis of Acrylamide, a Carcinogen Formed in Heated Foodstuffs Journal of Agricultural and Food Chemistry. ,vol. 50, pp. 4998- 5006 ,(2002) , 10.1021/JF020302F
E. Tareke, P. Rydberg, P. Karlsson, S. Eriksson, M. Törnqvist, Acrylamide: A Cooking Carcinogen? Chemical Research in Toxicology. ,vol. 13, pp. 517- 522 ,(2000) , 10.1021/TX9901938
Laurence Castle, Maria-Jesus Campos, John Gilbert, Determination of acrylamide monomer in hydroponically grown tomato fruits by capillary gas chromatography-mass spectrometry Journal of the Science of Food and Agriculture. ,vol. 54, pp. 549- 555 ,(1991) , 10.1002/JSFA.2740540406
Laurence. Castle, Determination of acrylamide monomer in mushrooms grown on polyacrylamide gel Journal of Agricultural and Food Chemistry. ,vol. 41, pp. 1261- 1263 ,(1993) , 10.1021/JF00032A019
L. S. Bologna, F. F. Andrawes, F. W. Barvenik, R. D. Lentz, R. E. Sojka, Analysis of Residual Acrylamide In Field Crops Journal of Chromatographic Science. ,vol. 37, pp. 240- 244 ,(1999) , 10.1093/CHROMSCI/37.7.240