Rapid separation of nanodiamond particles by viscosity gradient centrifugation

作者: Jiaying Qu , Jean Felix Mukerabigwi , Nianshun Yang , Xueying Huang , Yuyang Sun

DOI: 10.1007/S13204-020-01568-8

关键词:

摘要: The nanodiamond (ND) particles have several potential applications including tribology, drug delivery, bioimaging, etc. However, the severe colloidal aggregation tendency of ND strictly limits its exploitation. Moreover, due to NDs rich surface chemistry and relatively small size, it is still difficult separate these large using conventional separation methods. Herein, we develop an efficient straightforward strategy aminated nanodiamonds (ND-NH2) into size nanoparticles by viscosity gradient centrifugation method in a polyvinylpyrrolidone (PVP) aqueous solution. Prior after separation, pristine ND-NH2 morphology were characterized DLS (dynamic light scattering analyzer) TEM (transmission electron microscopic), which show that with narrow distribution uniform can be easily separated PVP This simple, rapid effective could extended other functionalized different sizes.

参考文章(51)
C. A. Price, Eric F. Eikenberry, Centrifugation in Density Gradients ,(1982)
Vadym N. Mochalin, Yury Gogotsi, Nanodiamond-Polymer Composites Diamond and Related Materials. ,vol. 58, pp. 161- 171 ,(2015) , 10.1016/J.DIAMOND.2015.07.003
RAE ZIMMERMAN, After the Deluge Sciences-new York. ,vol. 34, pp. 18- 23 ,(1994) , 10.1002/J.2326-1951.1994.TB03770.X
Kristopher D. Behler, Antonella Stravato, Vadym Mochalin, Guzeliya Korneva, Gleb Yushin, Yury Gogotsi, Nanodiamond-Polymer Composite Fibers and Coatings ACS Nano. ,vol. 3, pp. 363- 369 ,(2009) , 10.1021/NN800445Z
Xin-Ling Tang, Peng Jiang, Guang-Lu Ge, Masaharu Tsuji, Si-Shen Xie, Yan-Jun Guo, Poly(N-vinyl-2-pyrrolidone) (PVP)-Capped Dendritic Gold Nanoparticles by a One-Step Hydrothermal Route and Their High SERS Effect Langmuir. ,vol. 24, pp. 1763- 1768 ,(2008) , 10.1021/LA703495S
Brian L. Cushing, Vladimir L. Kolesnichenko, Charles J. O'Connor, Recent advances in the liquid-phase syntheses of inorganic nanoparticles. Chemical Reviews. ,vol. 104, pp. 3893- 3946 ,(2004) , 10.1021/CR030027B
Matthias Hanauer, Sebastien Pierrat, Inga Zins, Alexander Lotz, Carsten Sönnichsen, Separation of Nanoparticles by Gel Electrophoresis According to Size and Shape Nano Letters. ,vol. 7, pp. 2881- 2885 ,(2007) , 10.1021/NL071615Y
A. Krüger, F. Kataoka, M. Ozawa, T. Fujino, Y. Suzuki, A.E. Aleksenskii, A. Ya. Vul’, E. Ōsawa, Unusually tight aggregation in detonation nanodiamond: Identification and disintegration Carbon. ,vol. 43, pp. 1722- 1730 ,(2005) , 10.1016/J.CARBON.2005.02.020
Shouheng Sun, Christopher B Murray, Dieter Weller, Liesl Folks, Andreas Moser, Monodisperse FePt Nanoparticles and Ferromagnetic FePt Nanocrystal Superlattices Science. ,vol. 287, pp. 1989- 1992 ,(2000) , 10.1126/SCIENCE.287.5460.1989
Vadym N. Mochalin, Olga Shenderova, Dean Ho, Yury Gogotsi, The properties and applications of nanodiamonds Nature Nanotechnology. ,vol. 7, pp. 11- 23 ,(2012) , 10.1038/NNANO.2011.209