Synthesis and characterization of some PLNZT ceramics

作者: Dev K. Mahato , R. K. Chaudhary , A. K. Bhattamishra , S. C. Srivastava

DOI: 10.1023/B:JMSE.0000036035.13186.37

关键词:

摘要: Powder of sodium doped polycrystalline samples PLZT with composition Pb-0.98(La1-x/3Nax)(0.02)(Zr-0.53 Ti-0.47)(0.9950) .O-3 (PLNZT) x = 0.5 was systematically prepared using spray drying technique. Rhombohedral phase PLNZT compound has been confirmed after being calcined at 800 degreesC. IDTA-TGA and XRD studies were used to characterize the synthesized. SEM for micro-structural evaluation. The dielectric constant (epsilon) loss tangent (tan delta) studied different temperatures 10 kHz frequency, which suggests that undergoes a ferro-electric transition diffuse type. (C) 2004 Kluwer Academic Publishers.

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