Structure of the O-specific polysaccharide from the deep-sea marine bacterium Idiomarina abyssalis КММ 227T containing a 2-O-sulfate-3-N-(4-hydroxybutanoyl)-3,6-dideoxy-d-glucose

作者: Maxim S. Kokoulin , Nadezhda A. Komandrova , Anatoly I. Kalinovskiy , Svetlana V. Tomshich , Lyudmila A. Romanenko

DOI: 10.1016/J.CARRES.2015.05.012

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摘要: Abstract The O-specific polysaccharide was isolated from the lipopolysaccharide of type strain Idiomarina abyssalis КММ 227T and studied by sugar analysis, Smith degradation, two-dimensional 1H 13C NMR spectroscopy including 1H,1H-TOCSY, 1H,1H-COSY, 1H,1H-ROESY, 1H,13C-HSQC, 1H,13C-HMBC, 1H,13C-H2BC 1H,13C-HSQC-TOCSY experiments. new structure I. abyssalis containing 2-O-sulfate-3-N-(4-hydroxybutanoyl)-3,6-dideoxy- d -glucose established: Download : full-size image

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