Dense and cellular zirconia produced by gel casting with agar: preparation and high temperature characterization

作者: Jean-Marc Tulliani , Edoardo Bemporad , Marco Sebastiani , Giovanni Pulci , Jacopo Tirillò

DOI: 10.1155/2013/108076

关键词:

摘要: A modified gel-casting process was developed to produce both dense and highly porous (40% volume) yttria tetragonal zirconia polycrystal (Y-TZP) using agar, a natural polysaccharide, as gelling agent. fugitive phase, made of commercial polyethylene spheres, added the ceramic suspension before cellular structures. The characterization microstructural features ceramics carried out by FEG SEM analysis cross-sections produced focused ion beam. mechanical properties components were characterized at room temperature nanoindentation tests in continuous stiffness measurement mode, investigating direct effect presence residual microporosity. diffuse microporosity from incomplete gel deaeration resulted decay bending strength elastic modulus. behavior (in terms modulus, flexural strength, deformation rupture) investigated performing four-point 1500°C.

参考文章(41)
P Sepulveda, Gelcasting foams for porous ceramics American Ceramic Society Bulletin. ,vol. 76, pp. 61- 65 ,(1997)
Jean-Marc Tulliani, Valentina Naglieri, Mariangela Lombardi, Laura Montanaro, Porous Alumina and Zirconia Bodies Obtained by a Novel Gel Casting Process The American Ceramic Society. ,vol. 29, pp. 327- 338 ,(2009) , 10.1002/9780470456262.CH28
Mariangela Lombardi, Laura Montanaro, Laurent Gremillard, Jrme Chevalier, A Modified Gelcasting Procedure to Prepare Alumina Porous Components: Process Optimization and Preliminary Mechanicals Tests 32nd International Conference on Advanced Ceramics and Composites. ,vol. 29, pp. 287- 297 ,(2009) , 10.1002/9780470456262.CH25
J.-M. Tulliani, M. Lombardi, P. Palmero, M. Fornabaio, L.J. Gibson, Development and mechanical characterization of novel ceramic foams fabricated by gel-casting Journal of The European Ceramic Society. ,vol. 33, pp. 1567- 1576 ,(2013) , 10.1016/J.JEURCERAMSOC.2013.01.038
F.S. Ortega, F.A.O. Valenzuela, C.H. Scuracchio, V.C. Pandolfelli, Alternative gelling agents for the gelcasting of ceramic foams Journal of The European Ceramic Society. ,vol. 23, pp. 75- 80 ,(2003) , 10.1016/S0955-2219(02)00075-4
Jin Feng Wang, Xiao Qing Wang, Wei Zhao, Alumina Gelcasting by Using Glutin-Urea System Advanced Materials Research. pp. 1423- 1426 ,(2011) , 10.4028/WWW.SCIENTIFIC.NET/AMR.284-286.1423
Deyu Kong, Hui Yang, Su Wei, Dongyun Li, Jiabang Wang, Gel-casting without de-airing process using silica sol as a binder Ceramics International. ,vol. 33, pp. 133- 139 ,(2007) , 10.1016/J.CERAMINT.2005.08.006
O. Şahin, O. Uzun, U. Kölemen, N. Uçar, Mechanical characterization for β-Sn single crystals using nanoindentation tests Materials Characterization. ,vol. 59, pp. 427- 434 ,(2008) , 10.1016/J.MATCHAR.2007.02.016
V.M. Kevorkijan, An ideal reinforcement for structural composites American Ceramic Society Bulletin. ,vol. 76, pp. 61- 67 ,(1997)