Synthesis of substituted heterocyclic cyclophanes

作者: W. Ried , S. Aboul-Fetouh

DOI: 10.1016/S0040-4020(01)85975-5

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摘要: Abstract The reaction of 1,2-bis-(5-tetrazolyl)benzene or 1,2-bis-(5-tetrazo1y1)pyrazines with dibromoalkane in the presence triethylamine gave corresponding symmetric and asymmetric cycophanes. structure which was partially characterized by spectral (infrared, 1H-nmr) methods fully elucidated single crystal X-ray analysis.

参考文章(5)
P. Scheiner, E. Stockel, D. Cruset, R. Noto, Ditetrazolylbenzene dianions. Potential precursors of the phenylenedimethylenes The Journal of Organic Chemistry. ,vol. 37, pp. 4207- 4209 ,(1972) , 10.1021/JO00798A061
William G. Finnegan, Ronald A. Henry, Robert Lofquist, An Improved Synthesis of 5-Substituted Tetrazoles Journal of the American Chemical Society. ,vol. 80, pp. 3908- 3911 ,(1958) , 10.1021/JA01548A028
Ronald A. Henry, Methylation of 5-Phenyltetrazole Journal of the American Chemical Society. ,vol. 73, pp. 4470- 4470 ,(1951) , 10.1021/JA01153A517
Bill Elpern, The Dialkylaminoalkylation of Some 5-Monosubstituted Tetrazoles Journal of the American Chemical Society. ,vol. 75, pp. 661- 662 ,(1953) , 10.1021/JA01099A044
Shin. Hayao, Herbert J. Havera, Wallace G. Strycker, T. J. Leipzig, Rodolfo. Rodriguez, New antihypertensive aminoalkyltetrazoles. Journal of Medicinal Chemistry. ,vol. 10, pp. 400- 402 ,(1967) , 10.1021/JM00315A025