Synthesis of single azo disperse dye containing double ester and determination of crystal structure
作者： Zhengyu Zhang , Hong Xu , Chunling Zheng
DOI: 10.1007/S11814-013-0167-8
关键词:
摘要: The synthesis, crystal structure analysis and characterization of a monoazo dye, 4-((2,6-dichloro-4-nitro phenyl)azo)-N-(diacetyl oxygen ethyl)aniline, are reported. dye crystallised in the triclinic system, space group P-1 with a=8.1663(3) A, b= 9.4222(3) c=15.4694(5) α=78.9130(10)°, β=75.019(2)°, γ=70.787(2)°, V=1078.26(6) A3 Z=2. There is only one molecule asymmetric unit. dihedral angle between two phenyl rings 53.4 A. In structure, intermolecular C-H…O hydrogen bonds link molecules into centrosymmetric dimers, forming R22(30) ring motifs, which they may be effective stabilization structure. Between rings, π…π stacking (interactions) further stabilize
springer.com
cheric.org 参考文章(28)
Y QIAN, G WANG, G XIAO, B LIN, Y CUI, The first-order molecular hyperpolarizability and thermal stability of charge-transfer azo diol and azo aldimine Dyes and Pigments. ,vol. 75, pp. 460- 465 ,(2007) , 10.1016/J.DYEPIG.2006.06.029
Li Yuan, Guozheng Liang, JianQiang Xie, Lan Li, Jing Guo, Preparation and characterization of poly(urea-formaldehyde) microcapsules filled with epoxy resins Polymer. ,vol. 47, pp. 5338- 5349 ,(2006) , 10.1016/J.POLYMER.2006.05.051
Wen Yang, Xiu-Li You, Yong Zhong, De-Chun Zhang, The crystal structure of 4-[(2-methoxy-4-nitro-phenylazo)-phenyl]-dimethyl-amine Dyes and Pigments. ,vol. 73, pp. 317- 321 ,(2007) , 10.1016/J.DYEPIG.2005.11.013
Ji-Eun Lee, Hyun Jee Kim, Mi Ran Han, Su Yeon Lee, Won Joo Jo, Shim Sung Lee, Jeong Sook Lee, Crystal structures of C.I. Disperse Red 65 and C.I. Disperse Red 73 Dyes and Pigments. ,vol. 80, pp. 181- 186 ,(2009) , 10.1016/J.DYEPIG.2008.07.001
Herbert B. Scher, Marius Rodson, Kuo-Shin Lee, Microencapsulation of pesticides by interfacial polymerization utilizing isocyanate or aminoplast chemistry Pesticide Science. ,vol. 54, pp. 394- 400 ,(1998) , 10.1002/(SICI)1096-9063(199812)54:4<394::AID-PS829>3.0.CO;2-S
K SINGH, A MAHAJAN, W ROBINSON, Single crystal X-ray structure analysis of some heterocyclic monoazo disperse dyes Dyes and Pigments. ,vol. 74, pp. 95- 102 ,(2007) , 10.1016/J.DYEPIG.2006.01.018
M. Muruganandham, N. Shobana, M. Swaminathan, Optimization of solar photocatalytic degradation conditions of Reactive Yellow 14 azo dye in aqueous TiO2 Journal of Molecular Catalysis A-chemical. ,vol. 246, pp. 154- 161 ,(2006) , 10.1016/J.MOLCATA.2005.09.052
M Muruganandham, M Swaminathan, Solar photocatalytic degradation of a reactive azo dye in TiO2-suspension Solar Energy Materials and Solar Cells. ,vol. 81, pp. 439- 457 ,(2004) , 10.1016/J.SOLMAT.2003.11.022
Anhe Wang, Cheng Tao, Yue Cui, Li Duan, Yang Yang, Junbai Li, Assembly of environmental sensitive microcapsules of PNIPAAm and alginate acid and their application in drug release. Journal of Colloid and Interface Science. ,vol. 332, pp. 271- 279 ,(2009) , 10.1016/J.JCIS.2008.12.032
A. Ghanadzadeh, M.A. Shahzamanian, S. Shoarinejad, M.S. Zakerhamidi, M. Moghadam, Guest–host interaction of some aminoazobenzene dyes doped in liquid crystalline matrix Journal of Molecular Liquids. ,vol. 136, pp. 22- 28 ,(2007) , 10.1016/J.MOLLIQ.2007.01.012