Microgram scale determination of total lipid carbon in valuable sediments using a thin-layer chromatography/flame ionization detector analyzer
作者： Kazuko. Ogura , Masako. Ishimura , Junko. Hisatake
DOI: 10.1021/AC00136A011
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摘要: Rapid and small size analytical methods of extractable lipid carbon in sediments are presented by applying a thin-layer chromatography/flame ionization detection system (TLC/FID analyzer, Iatroscan TH-10), using silica-coated Chromarod without development. A minimum 60 samples total can be analyzed 10 min. The sample used averaged 2.5 ..mu..g carbon, with an allowable reproducibility (standard deviation +/- 10%). good correlation 1400-m core sediment Lake Biwa, is obtained both this method the wet oxidation method. has been developed modifying Menzel Vaccaro's method, which determination dissolved organic carbon.
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Kerry Fagan, John K. Pollak, The effect of the phenoxyacetic acid herbicides 2,4,5-trichlorophenoxyacetic acid and 2,4-dichlorophenoxyacetic acid as ascertained by direct experimentation Residue reviews. ,vol. 92, pp. 29- 58 ,(1984) , 10.1007/978-1-4612-5266-5_2
R.J. Pearce, Amino acid analysis by gas-liquid chromatography of N-heptafluorobutyryl isobutyl esters. Complete resolution using a support-coated open-tubular capillary column. Journal of Chromatography A. ,vol. 136, pp. 105- 111 ,(1977) , 10.1016/S0021-9673(00)83000-9
Kimitaka Kawamura, Ryoshi Ishiwatari, Experimental diagenesis of fatty acids in a sediment: Changes in their existence forms upon heating. Geochemical Journal. ,vol. 15, pp. 1- 8 ,(1981) , 10.2343/GEOCHEMJ.15.1
H. Read, Improved sample application methods for the Iatroscan Lipids. ,vol. 20, pp. 510- 515 ,(1985) , 10.1007/BF02534891
Kazuko OGURA, Concentrations of total lipids and their significance as an index of paleoclimates in the 200m long core sample of Lake Biwa. Proceedings of the Japan Academy. Ser. B: Physical and Biological Sciences. ,vol. 54, pp. 145- 150 ,(1978) , 10.2183/PJAB.54.145
C. C. Parrish, R. G. Ackman, The effect of developing solvents on lipid class quantification in chromarod thin layer chromatography/flame ionization detection Lipids. ,vol. 18, pp. 563- 565 ,(1983) , 10.1007/BF02535398
Masood Arjmand, Ralph O. Mumma, Metabolism of 2,4-dichlorophenoxyacetic acid. 8. Gas-liquid chromatography of trimethylsilyl derivatives of amino acid conjugates. Journal of Agricultural and Food Chemistry. ,vol. 24, pp. 574- 580 ,(1976) , 10.1021/JF60205A069
Wayne S. Gardner, William A. Frez, Elizabeth A. Cichocki, Christopher C. Parrish, Micromethod for lipids in aquatic invertebrates1 Limnology and Oceanography. ,vol. 30, pp. 1099- 1105 ,(1985) , 10.4319/LO.1985.30.5.1099
Roger P. Delmas, Christopher C. Parrish, Robert G. Ackman, Determination of lipid class concentrations in seawater by thin-layer chromatography with flame ionization detection Analytical Chemistry. ,vol. 56, pp. 1272- 1277 ,(1984) , 10.1021/AC00272A018
Ryoshi Ishiwatari, Kazuko Ogura, Shoji Horie, Organic geochemistry of a lacustrine sediment (Lake Haruna, Japan) Chemical Geology. ,vol. 29, pp. 261- 280 ,(1980) , 10.1016/0009-2541(80)90024-8