Synthesis, structural study, magnetic susceptibility and antimicrobial activity of the first (μ-oxo)-bis(oxalato)-vanadium(IV) 1D coordination polymer
作者： Hiba Sehimi , Badiaa Essghaier , Elisa Barea , Najla Sadfi-Zouaoui , Mohamed Faouzi Zid
DOI: 10.1016/J.MOLSTRUC.2018.08.053
关键词:
摘要: Abstract Catena-poly[bis(guanidinium) (μ-oxo)-bis(oxalato)-vanadium(IV)], 1, a new 1D polymeric V(IV) salt has been synthesized by slow evaporation at room temperature and its structure elucidated single-crystal X-ray diffraction, while bis [4-(dimethylamino)-pyridinium] aquabis (oxalato)oxidovanadate(IV) dihydrate's structure, 2, previously reported. In addition to elemental analysis, single crystal diffraction structural data report of both compounds 1 2 have characterized by, FT-IR UV–Vis spectroscopy, Rietveld refinement, TG–DSC analysis. Magnetic susceptibility the had investigated discussed in context their structures. The stability, availability ease synthesis those are an advantage for antimicrobial activity investigation against different Gram-positive Gram-negative bacteria, yeast fungi microorganisms. Further investigations on compounds' lysozyme spore germination inhibition aim go deeper mechanism actions.
sci-hub.se 参考文章(39)
Chen Chen, Cao Yun-zhu, Xing Yong-heng, Ren Dong-xue, Vanadium Haloperoxidases Model Compounds: Synthesis, Structural Characterization and Mimic Catalytic Bromination Activity of [VO(C2O4)(2,2′-bipy)(H2O)]．C2H5OH and VO(C2O4)(phen)(H2O) Chemical Research in Chinese Universities. ,vol. 28, pp. 768- 774 ,(2012)
J. R. Tagg, A. R. McGiven, Assay System for Bacteriocins Applied Microbiology. ,vol. 21, pp. 943- 943 ,(1971) , 10.1128/AM.21.5.943-943.1971
Akram Hamidi, Leila Hassani, Fakhrossadat Mohammadi, Parisa Jahangoshayi, Khosro Mohammadi, The biological effects of vanadyl curcumin and vanadyl diacetylcurcumin complexes: the effect on structure, function and oxidative stability of the peroxidase enzyme, antibacterial activity and cytotoxic effect. Journal of Enzyme Inhibition and Medicinal Chemistry. ,vol. 31, pp. 1124- 1131 ,(2016) , 10.3109/14756366.2015.1101091
Angelos M. Evangelou, Vanadium in cancer treatment. Critical Reviews in Oncology Hematology. ,vol. 42, pp. 249- 265 ,(2002) , 10.1016/S1040-8428(01)00221-9
Saeed Ahmad, Anvarhusein A. Isab, Saqib Ali, Abdul Rahman Al-Arfaj, Perspectives in bioinorganic chemistry of some metal based therapeutic agents Polyhedron. ,vol. 25, pp. 1633- 1645 ,(2006) , 10.1016/J.POLY.2005.11.004
Louis J. Farrugia, WinGX and ORTEP for Windows: an update Journal of Applied Crystallography. ,vol. 45, pp. 849- 854 ,(2012) , 10.1107/S0021889812029111
Juan Rodríguez-Carvajal, Recent advances in magnetic structure determination by neutron powder diffraction Physica B: Condensed Matter. ,vol. 192, pp. 55- 69 ,(1993) , 10.1016/0921-4526(93)90108-I
Stephanie L. Castro, Marion E. Cass, Frederick J. Hollander, Stuart L. Bartley, Oxo-Vanadium(IV) Dimer of 3-Hydroxy-3-methylglutarate: X-ray Crystal Structure, Solid State Magnetism, and Solution Spectroscopy Inorganic Chemistry. ,vol. 34, pp. 466- 472 ,(1995) , 10.1021/IC00106A008
Biswajit Mukherjee, Balaram Patra, Sushmita Mahapatra, Pratik Banerjee, Amit Tiwari, Malay Chatterjee, Vanadium—an element of atypical biological significance Toxicology Letters. ,vol. 150, pp. 135- 143 ,(2004) , 10.1016/J.TOXLET.2004.01.009
Chen Chen, Feng-Ying Bai, Rui Zhang, Ge Song, Hui Shan, Na Xing, Yong-Heng Xing, Synthesis, structure, and catalytic bromination of supramolecular oxovanadium complexes containing oxalate Journal of Coordination Chemistry. ,vol. 66, pp. 671- 688 ,(2013) , 10.1080/00958972.2013.765561