Magnetic porous carbon based solid-phase extraction coupled with high performance liquid chromatography for the determination of neonicotinoid insecticides in environmental water and peanut milk samples
作者： Li Liu , Yunhui Hao , Xin Zhou , Chun Wang , Qiuhua Wu
DOI: 10.1039/C4AY02990A
关键词:
摘要: Magnetic ordered porous carbon (MOPC–ZSM-5) was synthesized using zeolite ZSM-5 as a template and sucrose source. It used magnetic solid-phase extraction adsorbent for the of four neonicotinoid insecticides (acetamiprid, imidacloprid, thiacloprid thiamethoxam) from river water peanut milk samples prior to high performance liquid chromatography–ultraviolet detection. The calibration curves in showed linearity 1.0 200.0 ng mL−1 thiamethoxam, 0.5 acetamiprid. For samples, observed range 6.0–1000.0 thiacloprid, 3.0–1000.0 acetamiprid, respectively. developed method has been successfully applied determination satisfactory result obtained.
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