Voltammetric determination of ibuprofen using a carbon paste – multiwalled carbon nanotube composite electrode

作者: Selene Irisais Rivera-Hernández , Giaan Arturo Álvarez-Romero , Silvia Corona-Avendaño , María Elena Páez-Hernández , Carlos Andrés Galán-Vidal

DOI: 10.1080/10739149.2016.1173061

关键词:

摘要: ABSTRACTAn optimized voltammetric method is reported for the quantification of ibuprofen in aqueous solution using a carbon paste–multiwalled nanotube composite as working electrode. The electrode preparation and experimental conditions were optimized; sensitivity 228.08 mA mol−1 L was obtained. limits detection 9.1 µM 25.5 µM, respectively, linear dynamic range extended from 2.36–242 µM. repeatability 5.35% expressed relative standard deviation. Using statistical analysis lower concentrations, limit reduced to 4.13 µM. employed tablets.

参考文章(23)
Alejandro Ansón Casaos, Nanotubos de carbono: Estructura porosa y sus implicaciones en el campo de la energía CSIC - Instituto de Carboquímica (ICB). ,(2005)
G. Geisslinger, K. Dietzel, D. Loew, O. Schuster, G. Rau, G. Lachmann, K. Brune, High-performance liquid chromatographic determination of ibuprofen, its metabolites and enantiomers in biological fluids Journal of Chromatography B: Biomedical Sciences and Applications. ,vol. 491, pp. 139- 149 ,(1989) , 10.1016/S0378-4347(00)82827-3
Ivan Švancara, Karel Vytřas, Kurt Kalcher, Alain Walcarius, Joseph Wang, Carbon Paste Electrodes in Facts, Numbers, and Notes: A Review on the Occasion of the 50‐Years Jubilee of Carbon Paste in Electrochemistry and Electroanalysis Electroanalysis. ,vol. 21, pp. 7- 28 ,(2009) , 10.1002/ELAN.200804340
Jana Sádecká, Miroslav Čakrt, Andrea Hercegová, Jozef Polonský, Ivan Skačáni, Determination of ibuprofen and naproxen in tablets. Journal of Pharmaceutical and Biomedical Analysis. ,vol. 25, pp. 881- 891 ,(2001) , 10.1016/S0731-7085(01)00374-0
Sidra Amin, M. Tahir Soomro, Najma Memon, Amber R. Solangi, Sirajuddin, Tahira Qureshi, Ali R. Behzad, Disposable screen printed graphite electrode for the direct electrochemical determination of ibuprofen in surface water Environmental Nanotechnology, Monitoring and Management. ,vol. 1, pp. 8- 13 ,(2014) , 10.1016/J.ENMM.2014.07.001
A.O. Santini, J.E. de Oliveira, H.R. Pezza, L. Pezza, A new potentiometric ibuprofenate ion sensor immobilized in a graphite matrix for determination of ibuprofen in tablets Microchemical Journal. ,vol. 84, pp. 44- 49 ,(2006) , 10.1016/J.MICROC.2006.04.007
Patricia C Damiani, Mariela Bearzotti, Miguel A Cabezón, Spectrofluorometric determination of ibuprofen in pharmaceutical formulations. Journal of Pharmaceutical and Biomedical Analysis. ,vol. 25, pp. 679- 683 ,(2001) , 10.1016/S0731-7085(00)00584-7
María Ramos Payán, Miguel Ángel Bello López, Rut Fernández-Torres, Juan Luis Pérez Bernal, Manuel Callejón Mochón, HPLC determination of ibuprofen, diclofenac and salicylic acid using hollow fiber-based liquid phase microextraction (HF-LPME) Analytica Chimica Acta. ,vol. 653, pp. 184- 190 ,(2009) , 10.1016/J.ACA.2009.09.018
Amanda B Lima, Eric O Faria, Rodrigo HO Montes, Rafael R Cunha, Eduardo M Richter, Rodrigo AA Munoz, Wallans TP dos Santos, None, Electrochemical Oxidation of Ibuprofen and Its Voltammetric Determination at a Boron‐Doped Diamond Electrode Electroanalysis. ,vol. 25, pp. 1585- 1588 ,(2013) , 10.1002/ELAN.201300014
Jean C. Tsao, Thomas S. Savage, High-Performance Liquid Chromatographic Determination of Ibuprofen in Bulk Drug and Tablets Drug Development and Industrial Pharmacy. ,vol. 11, pp. 1123- 1131 ,(1985) , 10.3109/03639048509055601