Comparison of J-integral methods for the characterization of tough polypropylene grades close to the glass transition temperature

作者: Anja Gosch , Florian J. Arbeiter , Michael Berer , Gerald Pinter

DOI: 10.1016/J.ENGFRACMECH.2018.06.002

关键词:

摘要: Abstract The fracture mechanical characterization of very tough Polypropylene at room temperature is great interest for many technical applications. Precision and validity obtained values can significantly be influenced by notching crack length determination, which has thoroughly been shown in literature. Additionally, the proximity to glass transition induce further uncertainties. aim this study compare different J-integral methods elastic plastic mechanics determine J-R curves tested materials. Methods consist classical multi-specimen, a single specimen method (load separation) statistical approach (Weibull). Specific data reduction procedures based on physical principles were applied reduce scattering achieve reliable values. In way, was achieved with critical verification used methods. Finally, determined toughness value showed good agreement surface texture inspected surfaces.

参考文章(39)
Gerald Pinter, Florian Arbeiter, Bernd Schrittesser, Andreas Frank, Michael Berer, Cyclic tests on cracked round bars as a quick tool to assess the long term behaviour of thermoplastics and elastomers Polymer Testing. ,vol. 45, pp. 83- 92 ,(2015) , 10.1016/J.POLYMERTESTING.2015.05.008
A van der Wal, J.J Mulder, H.A Thijs, R.J Gaymans, Fracture of polypropylene: 1. The effect of molecular weight and temperature at low and high test speed Polymer. ,vol. 39, pp. 5467- 5475 ,(1998) , 10.1016/S0032-3861(97)10278-6
P. Doshev, R. Lach, G. Lohse, A. Heuvelsland, W. Grellmann, H.-J. Radusch, Fracture characteristics and deformation behavior of heterophasic ethylene–propylene copolymers as a function of the dispersed phase composition Polymer. ,vol. 46, pp. 9411- 9422 ,(2005) , 10.1016/J.POLYMER.2005.07.029
Edgardo Santarelli, Patricia Frontini, The effects of specimen size and testing conditions on fracture toughness evaluation of polypropylene homopolymer Polymer Engineering and Science. ,vol. 41, pp. 1803- 1814 ,(2001) , 10.1002/PEN.10877
B. Fayolle, A. Tcharkhtchi, J. Verdu, Temperature and molecular weight dependence of fracture behaviour of polypropylene films Polymer Testing. ,vol. 23, pp. 939- 947 ,(2004) , 10.1016/J.POLYMERTESTING.2004.04.013
R. Lach, S. Seidler, W. Grellmann, Resistance Against the Intrinsic Rate of Fracture Mechanics Parameters for Polymeric Materials Under Moderate Impact Loading Mechanics of Time-Dependent Materials. ,vol. 9, pp. 103- 119 ,(2005) , 10.1007/S11043-005-1084-Y
Wolfgang Grellmann, Sabine Seidler, Kerstin Jung, Ines Kotter, Crack‐resistance behavior of polypropylene copolymers Journal of Applied Polymer Science. ,vol. 79, pp. 2317- 2325 ,(2001) , 10.1002/1097-4628(20010328)79:13<2317::AID-APP1039>3.0.CO;2-N
A. Salazar, P.M. Frontini, J. Rodríguez, Determination of fracture toughness of propylene polymers at different operating temperatures Engineering Fracture Mechanics. ,vol. 126, pp. 87- 107 ,(2014) , 10.1016/J.ENGFRACMECH.2014.04.023