Preparation, crystal structure and infrared spectra of cis-[Pd (NH3) 2 (CN) 2]

摘要: ' E PAA i 1 0 il , CR 5 AL 5 IRU IUEAUI ll F AR D setcтад оғ Page 1 XIII_0235 Глигор Јовановски ' E PAA i 1 0 il , CR 5 AL 5 IRU IUEAUI ll F AR D setcтад оғ eza一[Pd(N﹚}:{CH):1 il . Pe na vi č and B. Kane na " L.: " eo ry of C en er al and In organi e Chemi a try , Facu l ty of 5 eia ne e . Un i vara i ty of Zagreb Haa L . Šop tra ja nova , 6. Jo van c vs ki * and 3. Šop traja no v Faculty of Chan is try, Cyr i L ad la t : o di : a Uni vars i ty, Skopja In an at tempt to p ra pare the cyan i de * a na 1 o gue of the li au que lin R = d Sa lt ( V RS ) , IP d (lli ) , ] I PdCl , ) , fres hlypre pa redsoluti ons of | Pd ('ll ) , J Cl - and K || Pd (Cl) , 1 ere mixed in an e qui mol ar rat io . Afte " 3 tand i ng for se veral days , ne edle - li ke crys ta ls separa te d from the re acti on mi xture and were re crys ta ili 2 ed from in ot wa ter . I hey ga ve an in fra red spectrum (F i g. i ) in ichclearly showed the presence of NH3 and Cl group s . 000 202 2び60 | 1 2.LU 120 10 11…