作者: Peijun Cai , Zeheng Yang , Chenyi Wang , Yunle Gu , Yitai Qian
DOI: 10.1246/CL.2005.1360
关键词: Chemical engineering 、 Nanocrystal 、 X-ray photoelectron spectroscopy 、 Autoclave 、 Nitride 、 Atmospheric temperature range 、 Chemistry 、 Nanotechnology 、 Refractory metals
摘要: Mo 2 N nanocrystals were successfully synthesized through a simple reaction route. The synthesis was carried out in an autoclave the temperature range of 450-550 °C, using MoCl 5 and NaN 3 as reactants. Characterized by XRD, XPS, TEM, composition morphology products confirmed. This work contributes effective facile method for preparing refractory metal nitride.