Synthesis of nanostructural turbostratic and hexagonal boron nitride coatings on carbon fiber cloths by dip-coating
作者： Morteza Ghanbarian , Ehsan Taheri Nassaj , Arash Kariminejad
DOI: 10.1016/J.SURFCOAT.2016.01.011
关键词: Microstructure 、 Nitride 、 Boric acid 、 Crystallization 、 Materials science 、 Boron nitride 、 Dip-coating 、 Nitriding 、 Coating 、 Composite material
摘要: Abstract The fabricating and characterization of boron nitride coating onto carbon fiber cloths via dip-coating process with boric acid urea as precursors, followed by nitriding in a nitrogen flow were done this study. Temperature cycles considered variables to find out optimum amounts. Dip-coating has 1, 2 4 cycles. Also, nitridation was different temperatures 650 1000 °C. results show that coatings exhibited pebble-like structure. SEM micrographs indicated the thickness nanostructural among 4 cycles is about 55, 120 210 nm, respectively. By increasing cycles, smoother surface developed. FT-IR XRD revealed film fabricated at 650 °C turbostratic microstructure nitridating temperature 1000 °C, hexagonal phase through film. Thermal analysis crystallization starts 600 °C.
sci-hub.se 参考文章(22)
Xiaopeng Hao, Meiyan Yu, Deliang Cui, Xiangang Xu, Qilong Wang, Minhua Jiang, The effect of temperature on the synthesis of BN nanocrystals Journal of Crystal Growth. ,vol. 241, pp. 124- 128 ,(2002) , 10.1016/S0022-0248(02)01291-5
Jože Grdadolnik, Yves Maréchal, Urea and urea–water solutions—an infrared study Journal of Molecular Structure. ,vol. 615, pp. 177- 189 ,(2002) , 10.1016/S0022-2860(02)00214-4
N. Murdie, C.P. Ju, J. Don, F.A. Fortunato, Microstructure of worn pitch/resin /CVI C-C composites Carbon. ,vol. 29, pp. 335- 342 ,(1991) , 10.1016/0008-6223(91)90202-T
R. Pankajavalli, S. Anthonysamy, K. Ananthasivan, P.R. Vasudeva Rao, Vapour pressure and standard enthalpy of sublimation of H3BO3 Journal of Nuclear Materials. ,vol. 362, pp. 128- 131 ,(2007) , 10.1016/J.JNUCMAT.2006.12.025
Takashi Sugino, Kazuhiko Tanioka, Seiji Kawasaki, Junji Shirafuji, Electron emission from nanocrystalline boron nitride films synthesized by plasma-assisted chemical vapor deposition Diamond and Related Materials. ,vol. 7, pp. 632- 635 ,(1998) , 10.1016/S0925-9635(97)00289-6
Yu Zheng, Shubin Wang, Synthesis of boron nitride coatings on quartz fibers: Thickness control and mechanism research Applied Surface Science. ,vol. 257, pp. 10752- 10757 ,(2011) , 10.1016/J.APSUSC.2011.07.092
L. Duclaux, B. Nysten, J-P. Issi, A. W. Moore, Structure and Low-temperature Thermal-conductivity of Pyrolytic Boron-nitride Physical Review B. ,vol. 46, pp. 3362- 3367 ,(1992) , 10.1103/PHYSREVB.46.3362
M DAS, S GHATAK, Synthesis of boron nitride from boron containing poly(vinyl alcohol) as ceramic precursor Bulletin of Materials Science. ,vol. 35, pp. 99- 102 ,(2012) , 10.1007/S12034-011-0248-4
P. Bergonzo, U. Kogelschatz, I.W. Boyd, Direct photo-deposition of silicon dioxide films using a xenon excimer lamp Applied Surface Science. ,vol. 69, pp. 393- 397 ,(1993) , 10.1016/0169-4332(93)90540-R
Xinmei Hou, Ziyou Yu, Kuo-Chih Chou, Facile synthesis of hexagonal boron nitride fibers with uniform morphology Ceramics International. ,vol. 39, pp. 6427- 6431 ,(2013) , 10.1016/J.CERAMINT.2013.01.070