Determination of carboxylic acids, sugars, glycerol and ethanol in wine and grape must by ion-exchange high-performance liquid chromatography with refractive index detection
作者： M. Calull , R.M. Marcé , F. Borrull
DOI: 10.1016/0021-9673(92)85384-6
关键词: Wine 、 Ion exchange 、 Malic acid 、 Carboxylic acid 、 Glycerol 、 Sugar 、 High-performance liquid chromatography 、 Ethanol 、 Chemistry 、 Chromatography 、 Organic chemistry 、 Analytical chemistry 、 Biochemistry 、 General Medicine
摘要: Method to determine the major carboxylic acids, sugars, glycerol and ethanol in wine grape must was developed using an ion-exchange column refractive index detector. A solid-phase extraction method with a strong anion exchanger used these compounds sweet wines musts. With this it is possible malic acid musts without interference from sugars. This high-performance liquid chromatographic compared standard methods of analysis. There good agreement accuracy precision methods.
elsevier.com
sci-hub.se 参考文章(11)
Jun Haginaka, Junko Wakai, Hiroyuki Yasuda, Tetsuo Nomura, Ion-exclusion chromatography of carboxylic acids with conductivity detection Peak enhancement using a cation-exchange hollow-fibre membrane and an alkaline solution Journal of Chromatography A. ,vol. 447, pp. 373- 382 ,(1988) , 10.1016/0021-9673(88)90047-7
Federica Caccamo, Guia Carfagnini, Antonio Di Corcia, Roberto Samperi, Improved high-performance liquid chromatographic assay for determining organic acids in wines Journal of Chromatography A. ,vol. 362, pp. 47- 53 ,(1986) , 10.1016/S0021-9673(01)86949-1
D. Tusseau, C. Benoit, Routine high-performance liquid chromatographic determination of carboxylic acids in wines and champagne. Journal of Chromatography A. ,vol. 395, pp. 323- 333 ,(1987) , 10.1016/S0021-9673(01)94121-4
E. Mentasti, M.C. Gennaro, C. Sarzanini, C. Baiocchi, M. Savigliano, Derivatization, identification and separation of carboxylic acids in wines and beverages by high-performance liquid chromatography. Journal of Chromatography A. ,vol. 322, pp. 177- 189 ,(1985) , 10.1016/S0021-9673(01)97670-8
R. Badoud, G. Pratz, Improved high-performance liquid chromatographic analysis of some carboxylic acids in food and beverages as their p-nitrobenzyl esters Journal of Chromatography A. ,vol. 360, pp. 119- 136 ,(1986) , 10.1016/S0021-9673(00)91656-X
R. M. Marcé, M. Calull, R. M. Manchobas, F. Borrull, F. X. Rius, An optimized direct method for the determination of carboxylic acids in beverages by HPLC Chromatographia. ,vol. 29, pp. 54- 58 ,(1990) , 10.1007/BF02261140
M. Calull, E. López, R.M. Marcé, J.C. Olucha, F. Borrull, Optimization of an ion-exchange high-performance liquid chromatographic method for the determination of carboxylic acids, sugars, glycerol and ethanol in wines Journal of Chromatography A. ,vol. 589, pp. 151- 158 ,(1992) , 10.1016/0021-9673(92)80016-N
Vincenzo Gerbi, M. Redoglia, A. Schneider, A Rapid HPLC Method for Separation and Determination of Major Organic Acids in Grape Musts and Wines American Journal of Enology and Viticulture. ,vol. 38, pp. 151- 155 ,(1987)
R. M. Marcé, M. Calull, F. X. Rius, F. Borrull, Determination of Major Carboxylic Acids in Wine by an Optimized HPLC Method with Linear Gradient Elution American Journal of Enology and Viticulture. ,vol. 41, pp. 289- 294 ,(1990)
Dewey D. Y. Ryu, J. D. McCord, E. Trousdale, An Improved Sample Preparation Procedure for the Analysis of Major Organic Components in Grape Must and Wine by High Performance Liquid Chromatography American Journal of Enology and Viticulture. ,vol. 35, pp. 28- 29 ,(1984)