Investigation of High-Temperature Stability and Thermal Endurance of Silicone Potting Compound by Thermo-Gravimetric Analysis
作者： Tanu Srivastava , Naresh Kumar Katari , Balaji Rao Ravuri , K. V. Govindrajan , S. Krishna Mohan
DOI: 10.1007/S12633-020-00725-6
关键词: Materials science 、 Silicone resin 、 Atmospheric temperature range 、 Degree (temperature) 、 Thermogravimetric analysis 、 Activation energy 、 Silicone 、 Potting 、 Composite material 、 Arrhenius equation
摘要: The high-temperature stability and thermal life of silicone resin-based potting compound (SC-3), used in the aerospace application for electrical insulation, is investigated Thermo-Gravimetry Analysis (TGA) an inert environment. Nonisothermal TGA performed temperature range 30 °C to 900 at 10, 20, / min heating rates. kinetic parameters such as activation energy pre-exponential factor are obtained by model-free method proposed Kissinger-Akahira-Sunose (KAS) Flynn Wall Ozawa (FWO) various degree conversion. degradation SC-3 observed 350 580 °C, endurance or time failure estimated per ASTM E1877 standard. results reveal that can be safely continuously 100 ~3.6 °C. Experimental also useful understand mechanism compound.
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Michael E. Brown, Introduction to Thermal Analysis: Techniques and applications ,(1988)
Philippe Cognard, Chapter 1 Introduction — how to use this handbook Handbook of Adhesives and Sealants. ,vol. 1, pp. 1- 20 ,(2005) , 10.1016/S1874-5695(02)80002-1
S Vyazovkin, Model-free kinetics Journal of Thermal Analysis and Calorimetry. ,vol. 83, pp. 45- 51 ,(2006) , 10.1007/S10973-005-7044-6
K. Chrissafis, Kinetics of thermal degradation of polymers Journal of Thermal Analysis and Calorimetry. ,vol. 95, pp. 273- 283 ,(2009) , 10.1007/S10973-008-9041-Z
S. Vyazovkin, Two types of uncertainty in the values of activation energy Journal of Thermal Analysis and Calorimetry. ,vol. 64, pp. 829- 835 ,(2001) , 10.1023/A:1011573218107
P. Budrugeac, E. Segal, Applicability of the Kissinger equation in thermal analysis Journal of Thermal Analysis and Calorimetry. ,vol. 88, pp. 703- 707 ,(2007) , 10.1007/S10973-006-8087-Z
S. N. Gladkikh, E. N. Basharina, O. L. Troitskaya, S. P. Kriulina, N. V. Timoshchenko, I. V. Nikitushkin, Development and Tests of Thermally Stable Potting and Impregnating Compounds Polymer Science. Series D. ,vol. 5, pp. 145- 149 ,(2012) , 10.1134/S1995421212030082
E. I. Alekseeva, S. R. Nanush’yan, I. Yu. Ruskol, E. V. Sokolyuk, Silicone compounds and sealants and their application in various branches of industry Polymer Science. Series D. ,vol. 3, pp. 244- 248 ,(2010) , 10.1134/S1995421210040076
Milena Marinović-Cincović, Bojan Janković, Vojislav Jovanović, Suzana Samaržija-Jovanović, Gordana Marković, The kinetic and thermodynamic analyses of non-isothermal degradation process of acrylonitrile―butadiene and ethylene―propylene―diene rubbers Composites Part B-engineering. ,vol. 45, pp. 321- 332 ,(2013) , 10.1016/J.COMPOSITESB.2012.08.006
Eung-Soo Kim, Hun-Sik Kim, Seong-Hun Jung, Jin-San Yoon, Adhesion properties and thermal degradation of silicone rubber Journal of Applied Polymer Science. ,vol. 103, pp. 2782- 2787 ,(2007) , 10.1002/APP.25402