Synthesis of nanocrystalline yttrium iron garnet by low temperature solid state reaction

作者: Hongtao Yu , Liwen Zeng , Chao Lu , Wenbo Zhang , Guangliang Xu

DOI: 10.1016/J.MATCHAR.2011.02.002

关键词: Yttrium iron garnetMaterials scienceGrain sizeAnalytical chemistrySinteringSaturation (magnetic)Nanocrystalline materialDifferential thermal analysisThermogravimetric analysisCeramicMineralogyMechanical engineeringGeneral Materials ScienceMechanics of MaterialsCondensed matter physics

摘要: Abstract In this work, nanocrystalline yttrium iron garnet powders were produced by low temperature solid state reaction. The phase evolution during the procedure was determined from thermogravimetric and differential thermal analysis, x-ray diffraction patterns. results of transmission electron microscopy indicated that prepared exhibited grain size at nano-level 20 ~ 40 nm. Dense ceramics with a theoretical density around 98% obtained after sintering 1280 °C, relative compared conventional ceramic processes, saturation magnetizations sintered samples also determined.

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