Gd-DTPA Adsorption on Chitosan/Magnetite Nanocomposites

作者: Ie. V. Pylypchuk , D. Kołodyńska , M. Kozioł , P. P. Gorbyk

DOI: 10.1186/S11671-016-1363-3

关键词: Nuclear chemistryChitosanSpecific surface areaMagnetiteLangmuirNanotechnologyDifferential thermal analysisMaterials scienceFreundlich equationAdsorptionFourier transform infrared spectroscopy

摘要: The synthesis of the chitosan/magnetite nanocomposites is presented. Composites were prepared by co-precipitation iron(II) and iron(III) salts aqueous ammonia in 0.1 % chitosan solution. It was shown that magnetite medium does not affect crystal structure. thermal analysis data showed 4.6 % mass concentration hybrid composite. In range initial Gd-DTPA solution up to 0.4 mmol/L, addition increases adsorption capacity affinity complex. Langmuir Freundlich models applied describe processes. Nanocomposites characterized scanning electron microscopy (SEM), differential (DTA), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), specific surface area determination (ASAP) methods.

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