Size control of monodisperse nonporous silica particles by seed particle growth

作者: Beibei Zhao , Caihua Tian , Yan Zhang , Tao Tang , Fengyun Wang

DOI: 10.1016/J.PARTIC.2010.07.028

关键词: DispersityMicrometreElectrolyteHydrolysisChemical engineeringParticle growthPorous mediumParticle sizeChromatographyMaterials scienceMultimodal distribution

摘要: Abstract Monodisperse nonporous silica particles were prepared by sol-precipitation via seed particle growth method, and the size, which varied from 1.0 to 4.7 μm, was strictly controlled in our experiment. The formation of secondary particles, resulted a multimodal distribution suppressed changing tetraethoxysilane (TEOS) concentration reaction temperature. Furthermore, effect adding small amounts electrolyte hydrolysis mixture examined.

参考文章(11)
Shakeel Ahmed, Syed A. Ali, Halim Hamid, Kosaku Honna, 61 Preparation, characterization, and catalytic evaluation of first stage hydrocracking catalyst Studies in Surface Science and Catalysis. ,vol. 145, pp. 295- 298 ,(2003) , 10.1016/S0167-2991(03)80218-5
Toshiyuki Kani, Takahiro Suzuki, Mayumi Tsukada, Hidehiro Kamiya, Influence of surface-adhered nanoparticles and nanoporous structure on bulk flowability of silica Powder Technology. ,vol. 176, pp. 108- 113 ,(2007) , 10.1016/J.POWTEC.2007.02.005
Jozua Laven, Hans N. Stein, The Electroviscous Behavior of Aqueous Dispersions of Amorphous Silica (Ludox). Journal of Colloid and Interface Science. ,vol. 238, pp. 8- 15 ,(2001) , 10.1006/JCIS.2001.7452
I.A. Rahman, P. Vejayakumaran, C.S. Sipaut, J. Ismail, M. Abu Bakar, R. Adnan, C.K. Chee, Effect of anion electrolytes on the formation of silica nanoparticles via the sol–gel process Ceramics International. ,vol. 32, pp. 691- 699 ,(2006) , 10.1016/J.CERAMINT.2005.05.004
Sung-Soo Kim, Hyun-Seok Kim, Sun Geon Kim, Woo-Sik Kim, Effect of electrolyte additives on sol-precipitated nano silica particles Ceramics International. ,vol. 30, pp. 171- 175 ,(2004) , 10.1016/S0272-8842(03)00085-3
Kyung-Soo Kim, Jun-Kyung Kim, Woo-Sik Kim, Influence of reaction conditions on sol-precipitation process producing silicon oxide particles Ceramics International. ,vol. 28, pp. 187- 194 ,(2002) , 10.1016/S0272-8842(01)00076-1
Zbigniew Adamczyk, Barbara Jachimska, Marta Kolasińska, Structure of colloid silica determined by viscosity measurements. joint international conference on information sciences. ,vol. 273, pp. 668- 674 ,(2004) , 10.1016/J.JCIS.2004.01.008
Sang Mok Chang, Minhyung Lee, Woo-Sik Kim, Preparation of large monodispersed spherical silica particles using seed particle growth. Journal of Colloid and Interface Science. ,vol. 286, pp. 536- 542 ,(2005) , 10.1016/J.JCIS.2005.01.059
T Issaeva, A Kourganov, K Unger, Super-high-speed liquid chromatography of proteins and peptides on non-porous Micra NPS-RP packings Journal of Chromatography A. ,vol. 846, pp. 13- 23 ,(1999) , 10.1016/S0021-9673(99)00360-X
C.G. Tan, B.D. Bowen, N. Epstein, Production of monodisperse colloidal silica spheres: Effect of temperature joint international conference on information sciences. ,vol. 118, pp. 290- 293 ,(1987) , 10.1016/0021-9797(87)90458-9