作者: Daniel H. Bechetti , John N. Dupont , Masashi Watanabe , John J. de Barbadillo
DOI: 10.1007/S11661-016-3952-2
关键词: Electron microscope 、 Inconel 、 Metallurgy 、 Alloy 、 Characterization (materials science) 、 Materials science 、 Electron backscatter diffraction 、 Grain boundary 、 Scanning transmission electron microscopy 、 Scanning electron microscope
摘要: Characterization of γ′ coarsened zones (CZs) in alloy 740H fusion welds via a variety electron microscopy techniques was conducted. The effects solute partitioning during nonequilibrium solidification on the amount strengthening precipitates along grain boundaries were evaluated electron-probe microanalysis and scanning microscopy. Electron backscatter diffraction used to present evidence for preferential growth CZs toward regions lower content, even if that direction increases boundary area. Scanning image analysis quantify propensity develop certain segments boundaries, as governed by local variations content. transmission with X-ray energy-dispersive spectrometry (XEDS) assess compositions matrix precipitate phases within segregation alloying components reaction front. Thermodynamic kinetic modeling compare calculated experimental compositions. work presented here provides new insight into progression discontinuous coarsening (DC) complex engineering alloy.