作者: Hideyuki Hirazawa , Satoshi Kusamoto , Hiromichi Aono , Takashi Naohara , Kensaku Mori
DOI: 10.1016/J.JALLCOM.2007.07.024
关键词: Crystal structure 、 Particle size 、 Orthorhombic crystal system 、 Cubic crystal system 、 Heat generation 、 Nuclear magnetic resonance 、 Calcination 、 Coprecipitation 、 Chemistry 、 Ferrite (magnet) 、 Analytical chemistry
摘要: Abstract New magnetic materials having a potentially high heat generation ability in an ac field were studied for application thermal coagulation therapy. The Mg 1− X Ca Fe 2 O 4 ferrites with varied from 0 to 1.0 synthesized using reverse coprecipitation method. obtained precursors calcined at various temperatures the range of 300–1000 °C intent obtain fine ferrite powders. was very poor = 0. However, improved partial 2+ substitution sites. maximum rise temperature (Δ T ) (370 kHz, 1.77 kA/m) ca. 50 °C samples 1.0 g weight and 0.2–0.8 . Especially, 800 °C showed highest generation. When -substituted 900 °C, reduced due decomposition into two phases MgFe -type cubic CaFe orthorhombic. In addition, 300 °C also Although crystal particle sizes increased calcination temperature, they did not influence this system. closely related hysteresis loss. reason properties 300 is ascribed increase loss by distortion structure.