Preparation of stochiometric CuInS 2 nanostructures by ultrasonic method

作者: M. Mousavi-Kamazani , M. Salavati-Niasari , H. Emadi

DOI: 10.1049/MNL.2012.0393

关键词: PhotoluminescenceX-ray crystallographyNanoparticleNanostructureUltrasonic sensorTransmission electron microscopyScanning electron microscopeParticle sizeAnalytical chemistryMaterials science

摘要: In this Letter, an ultrasonic method for the synthesis of CuInS2 nanostructure with use no surfactants is described. This facile and provides appropriate condition preparation structures various morphologies. study, effect different parameters such as type sulphur sources, concentration precursors, time power irradiation on morphology particle size were studied. The results indicated that source plays important role in CuInS2. synthesised materials characterised by means X-ray diffraction, energy-dispersive analysis, scanning electron microscopy, transmission infrared spectrum photoluminescence spectroscopy. nanoparticles obtained after calcinations products at 350°C. are discussed detail.

参考文章(31)
Xiaogang Peng, Liberato Manna, Weidong Yang, Juanita Wickham, Erik Scher, Andreas Kadavanich, A. P. Alivisatos, Shape control of CdSe nanocrystals Nature. ,vol. 404, pp. 59- 61 ,(2000) , 10.1038/35003535
Kenneth S. Suslick, Mingming Fang, Taeghwan Hyeon, Sonochemical Synthesis of Iron Colloids Journal of the American Chemical Society. ,vol. 118, pp. 11960- 11961 ,(1996) , 10.1021/JA961807N
Kulbinder K. Banger, Jennifer A. Hollingsworth, Jerry D. Harris, Jonathan Cowen, William E. Buhro, Aloysius F. Hepp, Ternary single-source precursors for polycrystalline thin-film solar cells Applied Organometallic Chemistry. ,vol. 16, pp. 617- 627 ,(2002) , 10.1002/AOC.362
Shengjie Peng, Fangyi Cheng, Jing Liang, Zhanliang Tao, Jun Chen, Facile solution-controlled growth of CuInS2 thin films on FTO and TiO2/FTO glass substrates for photovoltaic application Journal of Alloys and Compounds. ,vol. 481, pp. 786- 791 ,(2009) , 10.1016/J.JALLCOM.2009.03.084
Clemens Burda, Xiaobo Chen, Radha Narayanan, Mostafa A. El-Sayed, Chemistry and properties of nanocrystals of different shapes. Chemical Reviews. ,vol. 105, pp. 1025- 1102 ,(2005) , 10.1021/CR030063A
Manoj Nirmal, Louis Brus, Luminescence Photophysics in Semiconductor Nanocrystals Accounts of Chemical Research. ,vol. 32, pp. 407- 414 ,(1999) , 10.1021/AR9700320
Jianping Xiao, Yi Xie, Rui Tang, Yitai Qian, Synthesis and characterization of ternary CuInS2 nanorods via a hydrothermal route Journal of Solid State Chemistry. ,vol. 161, pp. 179- 183 ,(2001) , 10.1006/JSSC.2001.9247
Shikui Han, Mingguang Kong, Ying Guo, Mingtai Wang, Synthesis of copper indium sulfide nanoparticles by solvothermal method Materials Letters. ,vol. 63, pp. 1192- 1194 ,(2009) , 10.1016/J.MATLET.2009.02.032
Yunxia Chen, Xin He, Xiujian Zhao, Mingxia Song, Xingyong Gu, Preparation and characterization of copper indium disulfide films by facile chemical method Materials Science and Engineering: B. ,vol. 139, pp. 88- 94 ,(2007) , 10.1016/J.MSEB.2007.01.036